1,2,3,4-Tetrahydro-6-methoxy-1-phenylnaphthalene

Base Information

Chemical Name:1,2,3,4-Tetrahydro-6-methoxy-1-phenylnaphthalene
CAS No.:19353-88-9
Molecular Formula:C₁₇H₁₈O
Molecular Weight:238.329
Hs Code.:
DSSTox Substance ID:DTXSID901239964
ChEMBL ID:CHEMBL5181147

Synonyms:CHEMBL5181147;DTXSID901239964;BDBM50589798;1,2,3,4-Tetrahydro-6-methoxy-1-phenylnaphthalene;19353-88-9

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,3,4-Tetrahydro-6-methoxy-1-phenylnaphthalene

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:238.135765193
Heavy Atom Count:18
Complexity:256

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC2=C(C=C1)C(CCC2)C3=CC=CC=C3

Technology Process of 1,2,3,4-Tetrahydro-6-methoxy-1-phenylnaphthalene

There total 5 articles about 1,2,3,4-Tetrahydro-6-methoxy-1-phenylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 2844-82-8
methoxy-6, phenyl-1, dihydro-3,4 naphtalene

: 19353-88-9
6-methoxy-1-phenyl-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethanol; for 8h; under 2660 Torr;

Reference yield:

: 1078-19-9
6-methoxy-3,4-dihydro-1(2H)-naphthalenone

: 19353-88-9
6-methoxy-1-phenyl-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg / 1.) ether, 2.) a) RT, 6 h, b) reflux, 1 h

2: 77 percent / H₂ / PtO₂ / ethanol / 8 h / 2660 Torr

With hydrogen; magnesium; platinum(IV) oxide; In ethanol;

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 19353-88-9
6-methoxy-1-phenyl-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Mg / 2) Et₂O, 2h, reflux

2: conc. HCl / methanol / 0.67 h / Heating

3: H₂ / Pd/C / ethanol / Ambient temperature

With hydrogenchloride; hydrogen; magnesium; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1002/ardp.19903230106