N-(4'-cyanophenyl)-5-(4-cyano-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

Base Information

Chemical Name:N-(4'-cyanophenyl)-5-(4-cyano-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline
CAS No.:1538624-96-2
Molecular Formula:C₂₃H₁₈N₄O₄
Molecular Weight:414.42
Hs Code.:

Synonyms:N-(4'-cyanophenyl)-5-(4-cyano-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4'-cyanophenyl)-5-(4-cyano-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

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Technology Process of N-(4'-cyanophenyl)-5-(4-cyano-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

There total 3 articles about N-(4'-cyanophenyl)-5-(4-cyano-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1622438-23-6
C₂₄H₁₈N₄O₅

: 1538624-96-2
N-(4'-cyanophenyl)-5-(4-cyano-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

Guidance literature:: With lithium borohydride; In tetrahydrofuran; methanol; at 0 ℃; for 7h;
DOI:10.1016/j.bmcl.2014.07.011

Reference yield:

: 4198-90-7
3,5-dimethyl-4-hydroxybenzonitrile

: 1538624-96-2
N-(4'-cyanophenyl)-5-(4-cyano-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 120 °C

2: lithium borohydride / tetrahydrofuran; methanol / 7 h / 0 °C

With lithium borohydride; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.07.011

Reference yield:

: 1372129-84-4
5-chloro-N¹-(4-cyanophenyl)-4-methoxycarbonyl-2-nitroaniline

: 1538624-96-2
N-(4'-cyanophenyl)-5-(4-cyano-2,6-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 120 °C

2: lithium borohydride / tetrahydrofuran; methanol / 7 h / 0 °C

With lithium borohydride; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.07.011