(2,2-Dimethyl-6,7-diphenyl-2,3-dihydro-1H-pyrrolizin-5-yl)-essigsaeureethylester

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Chemical Name:(2,2-Dimethyl-6,7-diphenyl-2,3-dihydro-1H-pyrrolizin-5-yl)-essigsaeureethylester
CAS No.:116674-01-2
Molecular Formula:C₂₅H₂₇NO₂
Molecular Weight:373.495
Hs Code.:

Synonyms:(2,2-Dimethyl-6,7-diphenyl-2,3-dihydro-1H-pyrrolizin-5-yl)-essigsaeureethylester

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Chemical Property of (2,2-Dimethyl-6,7-diphenyl-2,3-dihydro-1H-pyrrolizin-5-yl)-essigsaeureethylester

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Technology Process of (2,2-Dimethyl-6,7-diphenyl-2,3-dihydro-1H-pyrrolizin-5-yl)-essigsaeureethylester

There total 6 articles about (2,2-Dimethyl-6,7-diphenyl-2,3-dihydro-1H-pyrrolizin-5-yl)-essigsaeureethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 623-73-4
diazoacetic acid ethyl ester

: 116673-96-2
2,2-Dimethyl-6,7-diphenyl-2,3-dihydro-1H-pyrrolizin

: 116674-01-2
(2,2-Dimethyl-6,7-diphenyl-2,3-dihydro-1H-pyrrolizin-5-yl)-essigsaeureethylester

Guidance literature:: With copper; In toluene; for 0.25h; Heating;
DOI:10.1002/ardp.19883210310

Reference yield:

: 116673-95-1
5-benzyl-3,3-dimethyl-3,4-dihydro-2H-pyrrole

: 116674-01-2
(2,2-Dimethyl-6,7-diphenyl-2,3-dihydro-1H-pyrrolizin-5-yl)-essigsaeureethylester

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / diethyl ether; ethanol; H₂O / 36 h / Ambient temperature

2: Cu / toluene / 0.25 h / Heating

With copper; sodium hydrogencarbonate; In diethyl ether; ethanol; water; toluene;
DOI:10.1021/jm00038a021

Reference yield:

: 70-11-1
α-bromoacetophenone

: 116674-01-2
(2,2-Dimethyl-6,7-diphenyl-2,3-dihydro-1H-pyrrolizin-5-yl)-essigsaeureethylester

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / diethyl ether; ethanol; H₂O / 36 h / Ambient temperature

2: Cu / toluene / 0.25 h / Heating

With copper; sodium hydrogencarbonate; In diethyl ether; ethanol; water; toluene;
DOI:10.1021/jm00038a021