C₂₇H₂₉ClN₂O₃

Base Information

Chemical Name:C₂₇H₂₉ClN₂O₃
CAS No.:1225208-84-3
Molecular Formula:C₂₇H₂₉ClN₂O₃
Molecular Weight:464.992
Hs Code.:

C<sub>27</sub>H<sub>29</sub>ClN<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₇H₂₉ClN₂O₃

Suppliers and Price of C₂₇H₂₉ClN₂O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₇H₂₉ClN₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₇H₂₉ClN₂O₃

There total 4 articles about C₂₇H₂₉ClN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.4%

: 7154-73-6
1-(2-aminoethyl)pyrrolidine

: 67632-03-5
3,4-bis(benzyloxy)-2-chlorobenzoic acid

: 1225208-84-3
C₂₇H₂₉ClN₂O₃

Guidance literature:: 3,4-bis(benzyloxy)-2-chlorobenzoic acid; With triethylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; at -15 ℃; for 1h; Inert atmosphere;

1-(2-aminoethyl)pyrrolidine; In tetrahydrofuran; for 2h; Inert atmosphere;

Reference yield:

: 32864-11-2
2-Chloro-3,4-dihydroxybenzaldehyde

: 1225208-84-3
C₂₇H₂₉ClN₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate; sodium iodide / N,N-dimethyl-formamide / 2 h / 40 °C / Inert atmosphere

2.1: sodium dihydrogenphosphate; sodium chlorite; water; dihydrogen peroxide / N,N-dimethyl-formamide / 3 h / 30 °C / Inert atmosphere

3.1: triethylamine; p-toluenesulfonyl chloride / tetrahydrofuran / 1 h / -15 °C / Inert atmosphere

3.2: 2 h / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; water; dihydrogen peroxide; sodium carbonate; triethylamine; p-toluenesulfonyl chloride; sodium iodide; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 5417-17-4
2-chloro-3,4-dimethoxybenzaldehyde

: 1225208-84-3
C₂₇H₂₉ClN₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride; pyridine / N,N-dimethyl acetamide / 5 h / 55 °C / Inert atmosphere; Reflux

2.1: sodium carbonate; sodium iodide / N,N-dimethyl-formamide / 2 h / 40 °C / Inert atmosphere

3.1: sodium dihydrogenphosphate; sodium chlorite; water; dihydrogen peroxide / N,N-dimethyl-formamide / 3 h / 30 °C / Inert atmosphere

4.1: triethylamine; p-toluenesulfonyl chloride / tetrahydrofuran / 1 h / -15 °C / Inert atmosphere

4.2: 2 h / Inert atmosphere

With pyridine; aluminum (III) chloride; sodium chlorite; sodium dihydrogenphosphate; water; dihydrogen peroxide; sodium carbonate; triethylamine; p-toluenesulfonyl chloride; sodium iodide; In tetrahydrofuran; N,N-dimethyl acetamide; N,N-dimethyl-formamide;