(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 2-oxophenylacetate

Base Information

Chemical Name:(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 2-oxophenylacetate
CAS No.:146499-04-9
Molecular Formula:C₂₇H₃₂O₄
Molecular Weight:420.549
Hs Code.:

Synonyms:(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 2-oxophenylacetate

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Chemical Property of (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 2-oxophenylacetate

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Technology Process of (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 2-oxophenylacetate

There total 1 articles about (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 2-oxophenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 25726-04-9
phenylglyoxylyl chloride

: 146499-02-7
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydro-1-naphthalenol

: 146499-04-9
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 2-oxophenylacetate

Guidance literature:: With pyridine; In benzene; for 3h;
DOI:10.1016/S0040-4020(01)80228-3

Reference yield: 100.0%

: 146499-04-9
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 2-oxophenylacetate

: (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl (R)-2-hydroxyphenylacetate

Guidance literature:: With diisobutylaluminium hydride; at -78 ℃;
DOI:10.1016/S0957-4166(00)86053-X

Reference yield:

: 146499-04-9
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 2-oxophenylacetate

: (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl (R)-2-hydroxyphenylacetate

: (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl (S)-2-hydroxyphenylacetate

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; at -78 ℃; for 0.25h; Product distribution; other reagent;
DOI:10.1016/S0040-4020(01)80228-3