(S)-1,2,4-TRIACETOXYBUTANE

Base Information

• Chemical Name: (S)-1,2,4-TRIACETOXYBUTANE
• CAS No.: 52067-45-5
• Molecular Formula: C₁₀H₁₆O₆
• Molecular Weight: 232.233
• Hs Code.: 2915390090
• Mol file: 52067-45-5.mol

Synonyms:1,2,4-BUTANETRIOL, TRIACETATE, (S);(S)-1,2,4-TRIACETOXYBUTANE

Chemical Property of (S)-1,2,4-TRIACETOXYBUTANE

Chemical Property:

• Boiling Point: 298.1±25.0 °C(Predicted)
• PSA: 78.90000
• Density: 1.136±0.06 g/cm3(Predicted)
• LogP: 0.43440

Purity/Quality:

98%Min ^*data from raw suppliers

(S)-1,2,4-TRIACETOXYBUTANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (S)-1,2,4-TRIACETOXYBUTANE

There total 4 articles about (S)-1,2,4-TRIACETOXYBUTANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(S)-1,2,4-butanetriol (42890-76-6,6810-31-7) + acetic anhydride (108-24-7) → (2S)-1,2,4-butanetriol (52067-45-5)

Guidance literature:

With pyridine; dmap; In dichloromethane; for 2h; Ambient temperature;

Reference yield:

methanol (67-56-1) + C46H62O14 + acetic anhydride (108-24-7) → (2S)-1,2,4-butanetriol (52067-45-5)

Guidance literature:

C₄₆H₆₂O₁₄; With ozone; In methanol; dichloromethane; at -78 ℃; for 0.583333h;

methanol; With sodium tetrahydroborate; In dichloromethane; at 0 ℃; for 0.5h;

acetic anhydride; With pyridine; at 20 ℃; for 11h;

DOI:10.1021/acs.orglett.9b01674

Reference yield:

acetic anhydride (108-24-7) + (2S,4S)-2,4-Dimethylpentan-1,3,5-triol (94842-97-4) → (2S)-1,2,4-butanetriol (52067-45-5)

Guidance literature:

In pyridine;

DOI:10.1002/hlca.19860690610

upstream raw materials:

(S)-1,2,4-butanetriol

acetic anhydride

(2S,4S)-2,4-Dimethylpentan-1,3,5-triol

methanol