2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2,4-di-O-benzyl-β-D-galactopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

Base Information

Chemical Name:2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2,4-di-O-benzyl-β-D-galactopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose
CAS No.:601493-47-4
Molecular Formula:C₆₁H₇₅N₅O₂₅
Molecular Weight:1278.28
Hs Code.:

2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2,4-di-O-benzyl-β-D-galactopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

Synonyms:2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2,4-di-O-benzyl-β-D-galactopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

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Chemical Property of 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2,4-di-O-benzyl-β-D-galactopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

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Technology Process of 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2,4-di-O-benzyl-β-D-galactopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

There total 1 articles about 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2,4-di-O-benzyl-β-D-galactopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: C₅₇H₇₁N₅O₂₃

: 601493-47-4
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2,4-di-O-benzyl-β-D-galactopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

Guidance literature:: With pyridine; dmap; at 20 ℃; for 14h;
DOI:10.1016/S0040-4020(03)00711-7

Reference yield: 96.0%

: 507-09-5
tiolacetic acid

: 601493-47-4
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2,4-di-O-benzyl-β-D-galactopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

: 601493-48-5
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2,4-di-O-benzyl-β-D-galactopyranosyl-(1->4)-2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-β-D-glucopyranose

Guidance literature:: With pyridine; at 20 ℃; for 24h;
DOI:10.1016/S0040-4020(03)00711-7

Reference yield:

: 601493-47-4
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2,4-di-O-benzyl-β-D-galactopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

: C₅₁H₆₇N₃O₂₀

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / pyridine / 24 h / 20 °C

2: sodium methoxide / methanol; tetrahydrofuran / 2 h / 20 °C

With pyridine; sodium methylate; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4020(03)00711-7