1-(3-hydroxyphenyl)-6-chloro-1,2,3,4-tetrahydro-β-carboline hydrochloride

Base Information

Chemical Name:1-(3-hydroxyphenyl)-6-chloro-1,2,3,4-tetrahydro-β-carboline hydrochloride
CAS No.:1236397-58-2
Molecular Formula:C₁₇H₁₅ClN₂O*ClH
Molecular Weight:335.233
Hs Code.:

Synonyms:1-(3-hydroxyphenyl)-6-chloro-1,2,3,4-tetrahydro-β-carboline hydrochloride

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Chemical Property of 1-(3-hydroxyphenyl)-6-chloro-1,2,3,4-tetrahydro-β-carboline hydrochloride

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Technology Process of 1-(3-hydroxyphenyl)-6-chloro-1,2,3,4-tetrahydro-β-carboline hydrochloride

There total 1 articles about 1-(3-hydroxyphenyl)-6-chloro-1,2,3,4-tetrahydro-β-carboline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.1%

: 942-26-7,55747-73-4
5-chlorotryptamine hydrochloride

: 100-83-4
meta-hydroxybenzaldehyde

: 1236397-58-2
1-(3-hydroxyphenyl)-6-chloro-1,2,3,4-tetrahydro-β-carboline hydrochloride

Guidance literature:: With acetic acid; at 95 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.05.024

Reference yield: 75.5%

: 1236397-58-2
1-(3-hydroxyphenyl)-6-chloro-1,2,3,4-tetrahydro-β-carboline hydrochloride

: 100-52-7
benzaldehyde

: 1236397-79-7
6-chloro-1-(3-hydroxyphenyl)-2-benzyl-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: With formic acid; potassium carbonate; In water; N,N-dimethyl-formamide; at 150 ℃; for 3h;
DOI:10.1016/j.bmc.2010.05.024

Reference yield: 69.3%

: 3744-87-4,7764-95-6,15761-38-3
N-t-butyloxycarbonyl-DL-alanine

: 1236397-58-2
1-(3-hydroxyphenyl)-6-chloro-1,2,3,4-tetrahydro-β-carboline hydrochloride

: 1236397-66-2
1-(3-hydroxyphenyl)-2-(α-(tert-butoxycarbonylamino)propionyl)-6-chloro-2,3,4,9-tetrahydrocarboline

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2010.05.024