D-MYO-INOSITOL 4-MONOPHOSPHATE AMMONIUM SALT

Base Information

• Chemical Name: D-MYO-INOSITOL 4-MONOPHOSPHATE AMMONIUM SALT
• CAS No.: 142760-33-6
• Molecular Formula: C₆H₁₃O₉P*2H₃N
• Molecular Weight: 294.199
• Mol file: 142760-33-6.mol

Synonyms:D-MYO-INOSITOL 4-MONOPHOSPHATE DIAMMONIUM SALT;D-myo-inositol 4-monophosphate ammonium;

Chemical Property of D-MYO-INOSITOL 4-MONOPHOSPHATE AMMONIUM SALT

Chemical Property:

• PSA: 180.55000
• LogP: -2.90320
• Storage Temp.: −20°C

Purity/Quality:

99% ^*data from raw suppliers

D-myo-Inositol-4-phosphate (ammonium salt) ≥98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of D-MYO-INOSITOL 4-MONOPHOSPHATE AMMONIUM SALT

There total 4 articles about D-MYO-INOSITOL 4-MONOPHOSPHATE AMMONIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-myo-inositol (87-89-8) → D-myo-inositol 1-phosphate diammonium salt (142760-33-6)

Guidance literature:

Multi-step reaction with 8 steps

1.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 11 h / Heating

1.2: 0.5 h / 0 °C

1.3: 11 h / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 20 °C

3.1: hydrogenchloride / water; dichloromethane; methanol / 18 h / 20 °C

4.1: 1H-tetrazole / dichloromethane / 24 h / 20 °C / Molecular sieve

4.2: 1 h / 0 °C / Molecular sieve

5.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 60 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

6.2: 4 h / 0 - 20 °C

7.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 40 °C

8.1: N,O-Bis(trimethylsilyl)trifluoroacetamide; trimethylsilyl bromide / dichloromethane; toluene / 1 h

8.2: 1 h / 0 - 20 °C

8.3: Dowex-1X₈ (HCO₃^-) resin

With 1H-imidazole; 1H-tetrazole; hydrogenchloride; trimethylsilyl bromide; tetrabutyl ammonium fluoride; N,O-Bis(trimethylsilyl)trifluoroacetamide; sodium hydride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil;

DOI:10.1039/c6ob01062h

Reference yield:

4,6-di-O-(para-methoxy-benzyl)-myo-inositol-1,3,5-orthoformate → D-myo-inositol 1-phosphate diammonium salt (142760-33-6)

Guidance literature:

Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 20 °C

2.1: hydrogenchloride / water; dichloromethane; methanol / 18 h / 20 °C

3.1: 1H-tetrazole / dichloromethane / 24 h / 20 °C / Molecular sieve

3.2: 1 h / 0 °C / Molecular sieve

4.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 60 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

5.2: 4 h / 0 - 20 °C

6.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 40 °C

7.1: N,O-Bis(trimethylsilyl)trifluoroacetamide; trimethylsilyl bromide / dichloromethane; toluene / 1 h

7.2: 1 h / 0 - 20 °C

7.3: Dowex-1X₈ (HCO₃^-) resin

With 1H-imidazole; 1H-tetrazole; hydrogenchloride; trimethylsilyl bromide; tetrabutyl ammonium fluoride; N,O-Bis(trimethylsilyl)trifluoroacetamide; sodium hydride; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil;

DOI:10.1039/c6ob01062h

Reference yield:

4,6-di-O-p-methoxybenzyl-2-O-methoxymethyl-D-myo-inositol 1,3,5-O-orthoformate → D-myo-inositol 1-phosphate diammonium salt (142760-33-6)

Guidance literature:

Multi-step reaction with 6 steps

1.1: hydrogenchloride / water; dichloromethane; methanol / 18 h / 20 °C

2.1: 1H-tetrazole / dichloromethane / 24 h / 20 °C / Molecular sieve

2.2: 1 h / 0 °C / Molecular sieve

3.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 60 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

4.2: 4 h / 0 - 20 °C

5.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 40 °C

6.1: N,O-Bis(trimethylsilyl)trifluoroacetamide; trimethylsilyl bromide / dichloromethane; toluene / 1 h

6.2: 1 h / 0 - 20 °C

6.3: Dowex-1X₈ (HCO₃^-) resin

With 1H-imidazole; 1H-tetrazole; hydrogenchloride; trimethylsilyl bromide; tetrabutyl ammonium fluoride; N,O-Bis(trimethylsilyl)trifluoroacetamide; sodium hydride; acetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil;

DOI:10.1039/c6ob01062h

upstream raw materials:

D-myo-inositol

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