zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer

Base Information

• Chemical Name: zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer
• CAS No.: 917596-91-9
• Molecular Formula: C₁₇₂H₂₄₂N₈O₈Si₂Zn₂
• Molecular Weight: 2736.81

Synonyms:zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer

Chemical Property of zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer

Chemical Property:

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Technology Process of zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer

There total 2 articles about zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl porphyrin (1054448-36-0) → zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer (917596-91-9)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine; p-benzoquinone; In toluene; at 20 ℃; Inert atmosphere;

DOI:10.1039/c4tc01120a

Reference yield:

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer (937026-89-6) → zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer (917596-91-9)

Guidance literature:

With tetramethylenediamine; CuCl; In dichloromethane; CuCl, TMEDA, CH2Cl2, O2 (n ->2n);

DOI:10.1021/ja067447d

Reference yield: 95.0%

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer (917596-91-9) → C172H246N8O8Si2

Guidance literature:

With trifluoroacetic acid; In chloroform; for 0.05h;

DOI:10.1039/c4tc01120a

upstream raw materials:

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl porphyrin

Downstream raw materials:

C₄H₉C₆H₄(C₂C₂₀H₈N₄Zn(C₆H₃(OC₈H₁₇)2)2C₂)2C₆H₄C₄H₉

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-ethynyl-porphyrin dimer

C₁₃₆H₁₆₆N₈O₈Zn₂

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