zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer

Base Information

• Chemical Name: zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer
• CAS No.: 937026-89-6
• Molecular Formula: C₁₅₄H₂₀₄N₈O₈SiZn₂
• Molecular Weight: 2454.23

Synonyms:zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer

Chemical Property of zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer

Chemical Property:

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Technology Process of zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer

There total 2 articles about zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer (917596-91-9) → zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer (937026-89-6)

Guidance literature:

With tetrabutylammonium fluoride; In dichloromethane; chloroform; 1. tetrabutylammonium fluoride, CH2Cl2:CHCl3 1:1; 2. separation;

DOI:10.1021/ja067447d

Reference yield:

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer (917596-91-9) → zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer (937026-89-6) + zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-ethynyl-porphyrin dimer (937026-98-7)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; chloroform; at 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1039/c4tc01120a

Reference yield: 26.0%

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10-ethynyl-20-trihexylsilanylethynyl-porphyrin dimer (937026-89-6) + zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-ethynyl-porphyrin dimer (937026-98-7) + N,N-dibutyl-4-iodo-1-aniline (90133-93-0) → C168H225N9O8SiZn2

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In toluene; at 50 ℃; for 2h; Schlenk technique; Inert atmosphere;

DOI:10.1039/c4tc01120a

upstream raw materials:

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer

Downstream raw materials:

zinc 5,15-bis-(3,5-bis-octyloxy-phenyl)-10,20-bis-trihexylsilanylethynyl-porphyrin dimer

(C₆H₁₃)3Si(C₂C₂₀H₈N₄Zn(C₆H₃(OC₈H₁₇)2)2C₂)2C₆H₄CHO

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