6-<4'-(tert-butoxycarbonyl)phenyl>-2-amino-3-cyano-3a,4,5,6a-tetrahydrothieno<2,3-b>pyrrole

Base Information

Chemical Name:6-<4'-(tert-butoxycarbonyl)phenyl>-2-amino-3-cyano-3a,4,5,6a-tetrahydrothieno<2,3-b>pyrrole
CAS No.:117098-12-1
Molecular Formula:C₁₈H₂₁N₃O₂S
Molecular Weight:343.45
Hs Code.:

Synonyms:6-<4'-(tert-butoxycarbonyl)phenyl>-2-amino-3-cyano-3a,4,5,6a-tetrahydrothieno<2,3-b>pyrrole

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Chemical Property of 6-<4'-(tert-butoxycarbonyl)phenyl>-2-amino-3-cyano-3a,4,5,6a-tetrahydrothieno<2,3-b>pyrrole

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Technology Process of 6-<4'-(tert-butoxycarbonyl)phenyl>-2-amino-3-cyano-3a,4,5,6a-tetrahydrothieno<2,3-b>pyrrole

There total 1 articles about 6-<4'-(tert-butoxycarbonyl)phenyl>-2-amino-3-cyano-3a,4,5,6a-tetrahydrothieno<2,3-b>pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 7357-70-2
Cyanothioacetamide

: 94930-27-5
1-<4-(tert-butyloxycarbonyl)phenyl>-3-pyrrolidinone

: 117098-12-1
6-<4'-(tert-butoxycarbonyl)phenyl>-2-amino-3-cyano-3a,4,5,6a-tetrahydrothieno<2,3-b>pyrrole

Guidance literature:: With acetic acid; 3-amino propanoic acid; In benzene; for 1.5h; Heating;
DOI:10.1021/jo00261a028

Reference yield:

: 117098-12-1
6-<4'-(tert-butoxycarbonyl)phenyl>-2-amino-3-cyano-3a,4,5,6a-tetrahydrothieno<2,3-b>pyrrole

: 117098-16-5
7-<4'-(tert-butoxycarbonyl)phenyl>-4-amino-4b,5,6,7a-tetrahydropyrrolo<3',2':4,5>thieno<2,3-d>pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulfonic acid / 1 h / 145 °C

2: NH₃ / ethanol / 48 h / 0 - 20 °C

With ammonia; toluene-4-sulfonic acid; In ethanol;
DOI:10.1021/jo00261a028