C₂₇H₃₂N₄O₁₄

Base Information

Chemical Name:C₂₇H₃₂N₄O₁₄
CAS No.:1374114-54-1
Molecular Formula:C₂₇H₃₂N₄O₁₄
Molecular Weight:636.569
Hs Code.:

C<sub>27</sub>H<sub>32</sub>N<sub>4</sub>O<sub>14</sub>

Synonyms:C₂₇H₃₂N₄O₁₄

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Chemical Property of C₂₇H₃₂N₄O₁₄

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Technology Process of C₂₇H₃₂N₄O₁₄

There total 4 articles about C₂₇H₃₂N₄O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 56932-42-4
5‐azido‐2‐hydroxybenzaldehyde

: 22900-11-4,100678-43-1,109121-98-4,109122-00-1,119241-60-0,119241-61-1,119241-62-2,20298-35-5
(2R,3R,4S)-3-acetamido-4-hydroxy-2-((1R,2R)-1,2,3-trihydroxypropyl)-3,4-dihydro-2H-pyran-6-carboxylic acid

: 75-36-5
acetyl chloride

: 1374114-54-1
C₂₇H₃₂N₄O₁₄

Guidance literature:: (2R,3R,4S)-3-acetamido-4-hydroxy-2-((1R,2R)-1,2,3-trihydroxypropyl)-3,4-dihydro-2H-pyran-6-carboxylic acid; acetyl chloride; at 20 ℃; for 36h; Inert atmosphere; Neat (no solvent);

5‐azido‐2‐hydroxybenzaldehyde; With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.02.001

Reference yield:

: 1374114-53-0
2-(1,3-dithian-2-yl)-4-nitrophenol

: 1374114-54-1
C₂₇H₃₂N₄O₁₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; zinc / 1 h / 20 °C

2.1: acetic acid; sodium nitrite / water / 2 h / 0 °C

2.2: 0.5 h / 0 - 20 °C

3.1: 36 h / 20 °C / Inert atmosphere; Neat (no solvent)

3.2: 24 h / 20 °C / Inert atmosphere

With acetic acid; zinc; sodium nitrite; In water;
DOI:10.1016/j.bmc.2012.02.001

Reference yield:

: C₁₀H₁₃NOS₂

: 1374114-54-1
C₂₇H₃₂N₄O₁₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; sodium nitrite / water / 2 h / 0 °C

1.2: 0.5 h / 0 - 20 °C

2.1: 36 h / 20 °C / Inert atmosphere; Neat (no solvent)

2.2: 24 h / 20 °C / Inert atmosphere

With acetic acid; sodium nitrite; In water;
DOI:10.1016/j.bmc.2012.02.001