4-N-DODECYLOXYBENZAMIDE

Base Information

• Chemical Name: 4-N-DODECYLOXYBENZAMIDE
• CAS No.: 179341-69-6
• Molecular Formula: C19H31NO2
• Molecular Weight: 305.461
• Mol file: 179341-69-6.mol

Synonyms:4-(Dodecyloxy)benzamide;

Chemical Property of 4-N-DODECYLOXYBENZAMIDE

Chemical Property:

• Vapor Pressure: 5.38E-08mmHg at 25°C
• Refractive Index: 1.503
• Boiling Point: 441.6 °C at 760 mmHg
• Flash Point: 140.1 °C
• PSA: 52.32000
• Density: 0.973 g/cm³
• LogP: 5.78550

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-N-DODECYLOXYBENZAMIDE

There total 4 articles about 4-N-DODECYLOXYBENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-(dodecyloxy)benzonitrile (29147-92-0) → 4-(dodecyloxy)benzamide (179341-69-6)

Guidance literature:

With sodium percarbonate; water; In acetone; at 50 ℃; for 9h;

DOI:10.1002/chem.200801408

Reference yield: 83.5%

p-hydroxybenzamide (619-57-8) + 1-dodecylbromide (143-15-7) → 4-(dodecyloxy)benzamide (179341-69-6)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; for 48h; Reflux;

DOI:10.1039/c9ra08211e

Reference yield: 70.0%

4-n-dodecyloxybenzaldehyde (24083-19-0) → 4-(dodecyloxy)benzamide (179341-69-6)

Guidance literature:

4-n-dodecyloxybenzaldehyde; With 9-aminofluorene; In toluene; at 20 ℃; for 0.5h;

With oxygen; triethylamine; In toluene; for 1.5h; Reflux;

DOI:10.1021/acs.orglett.6b02465

upstream raw materials:

1-Iodododecane

4-cyanophenol

4-(dodecyloxy)benzonitrile

4-n-dodecyloxybenzaldehyde

Downstream raw materials:

4-(dodecyloxy)aniline

Refernces

• 1、 Ghosh, Santanu,Jana, Chandan K.. "Aminofluorene-Mediated Biomimetic Domino Amination-Oxygenation of Aldehydes to Amides". supporting information. p. 5788 - 5791. Retrieved 2016/11/29.
• 2、 Ahn, Seokhoon,Morrison, Christine N.,Matzger, Adam J.. "Highly symmetric 2D rhombic nanoporous networks arising from low symmetry amphiphiles". supporting information; experimental part. p. 7946 - 7947. Retrieved 2009/12/02.