4-N-DODECYLOXYBENZALDEHYDE

Base Information

• Chemical Name: 4-N-DODECYLOXYBENZALDEHYDE
• CAS No.: 24083-19-0
• Molecular Formula: C19H30 O2
• Molecular Weight: 290.446
• Hs Code.: 2912499000
• Mol file: 24083-19-0.mol

Synonyms:Benzaldehyde,p-(dodecyloxy)- (8CI); 4-(Dodecyloxy)benzaldehyde; 4-n-Dodecyloxybenzaldehyde;p-(Dodecyloxy)benzaldehyde; p-(Lauryloxy)benzaldehyde

Chemical Property of 4-N-DODECYLOXYBENZALDEHYDE

Chemical Property:

• Appearance/Colour: slightly yellow to beige low melting solid
• Vapor Pressure: 7.31E-07mmHg at 25°C
• Melting Point: 25-28oC
• Refractive Index: 1.5360 (estimate)
• Boiling Point: 407.9°Cat760mmHg
• Flash Point: 157.1°C
• PSA: 26.30000
• Density: 0.947g/cm³
• LogP: 5.79880
• Sensitive.: Air Sensitive

Purity/Quality:

99% ^*data from raw suppliers

4-N-Dodecycloxybenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-N-DODECYLOXYBENZALDEHYDE

There total 13 articles about 4-N-DODECYLOXYBENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-hydroxy-benzaldehyde (123-08-0,65581-83-1) + 1-dodecylbromide (143-15-7) → 4-n-dodecyloxybenzaldehyde (24083-19-0)

Guidance literature:

4-hydroxy-benzaldehyde; With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 60 ℃; for 1h;

1-dodecylbromide; In N,N-dimethyl-formamide; at 80 ℃; Inert atmosphere;

DOI:10.1039/c6nj00634e

Reference yield: 83.0%

p-(dodecyloxy)benzyl alcohol (61440-63-9) → 4-n-dodecyloxybenzaldehyde (24083-19-0)

Guidance literature:

With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1016/S0040-4039(01)00169-1

Reference yield:

N,N'-Bis-[1-(4-dodecyloxy-phenyl)-meth-(E)-ylidene]-ethane-1,2-diamine → 4-n-dodecyloxybenzaldehyde (24083-19-0) + ethylenediamine (107-15-3,85404-18-8)

Guidance literature:

With 2-methyl-propan-1-ol; sulfuric acid; sodium dodecyl-sulfate; In hexane; water; at 27 ℃; Kinetics;

DOI:10.1002/kin.1042

upstream raw materials:

4-hydroxy-benzaldehyde

1-dodecylbromide

1-chlorododecane

1-bromo-4-dodecyloxybenzene

Downstream raw materials:

5,10,15,20-tetra(3-pyridyl)porphyrin

5,10,15-tri(3-pyridyl)-20-(4-dodecyloxyphenyl)porphin

5,15-di(3-pyridyl)-10,20-di(4-dodecyloxyphenyl)porphin

5-(3-pyridyl)-10,15,20-tri(4-dodecyloxyphenyl)porphin

Refernces

• 1、 Jamain, Zuhair,Khairuddean, Melati,Omar, Nor Faizawani. "Synthesis and determination of thermotropic liquid crystalline behavior of cinnamaldehyde-based molecules with two schiff base linking units". . . Retrieved 2020.
• 2、 Chen, Zhijian,Lei, Bin,Pan, Hongfei,Ren, Xiang-Kui,Zhang, Yongjie. "An amphiphilic B,O-chelated aza-BODIPY dye: synthesis, pH-sensitivity, and aggregation behaviour in a H2O/DMSO mixed solvent". . p. 6108 - 6114. Retrieved 2021.
• 3、 Bettoni, Marta,Brinchi, Lucia,Del Giacco, Tiziana,Germani, Raimondo,Meniconi, Sara,Rol, Cesare,Sebastiani, Giovanni Vittorio. "Surfactant effect on titanium dioxide photosensitized oxidation of 4-dodecyloxybenzyl alcohol". . p. 53 - 59. Retrieved 2012.
• 4、 De Witte, Pieter A. J.,Castriciano, Mariangela,Cornelissen, Jeroen J. L. M.,Scolaro, Luigi Monsu,Nolte, Roeland J. M.,Rowan, Alan E.. "Helical polymer-anchored porphyrin nanorods". . p. 1775 - 1781. Retrieved 2003.
• 5、 Xiao, Yuchuan,Cai, Fangjian,Peng, Xuan,Kang, Xiyuan,Lei, Peng,Li, Xin,Xu, Haijun,Xiao, Xunwen,Tu, Bin,Zeng, Qingdao. "Aza-BODIPY molecular assembly at the liquid-solid interface driven by Br?F[sbnd]BF interactions". supporting information. p. 3566 - 3569. Retrieved 2021/04/12.