Allyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside

Base Information

Chemical Name:Allyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside
CAS No.:137432-76-9
Molecular Formula:C₂₅H₂₉NO₆
Molecular Weight:439.508
Hs Code.:

Synonyms:Allyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside

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Chemical Property of Allyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside

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Technology Process of Allyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside

There total 6 articles about Allyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100-39-0
benzyl bromide

: 136845-44-8
Allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside

: 137432-76-9
Allyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside

Guidance literature:: With barium dihydroxide; barium(II) oxide; In N,N-dimethyl-formamide; for 4h; Ambient temperature;
DOI:10.1002/hlca.19920750505

Reference yield:

: 7512-17-6,72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4
N-Acetyl-D-glucosamine

: 137432-76-9
Allyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / BF₃*Et₂O / 4.5 h / 95 °C

2: 49 percent / ZnCl₂ / 19 h / Ambient temperature

3: NEt₃ / 0.83 h / 24 °C

4: 2-methoxyethanol, NaOAc / H₂O / 70 h / 118 °C

5: 92 percent / BaO, Ba(OH)2*8 H₂O / dimethylformamide / 3.75 h / 23 °C

With barium dihydroxide; 2-methoxy-ethanol; boron trifluoride diethyl etherate; sodium acetate; triethylamine; zinc(II) chloride; barium(II) oxide; In water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19910740625

Reference yield:

: 100-52-7
benzaldehyde

: 137432-76-9
Allyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 49 percent / ZnCl₂ / 19 h / Ambient temperature

2: NEt₃ / 0.83 h / 24 °C

3: 2-methoxyethanol, NaOAc / H₂O / 70 h / 118 °C

4: 92 percent / BaO, Ba(OH)2*8 H₂O / dimethylformamide / 3.75 h / 23 °C

With barium dihydroxide; 2-methoxy-ethanol; sodium acetate; triethylamine; zinc(II) chloride; barium(II) oxide; In water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19910740625