2-(3,4-dimethoxyphenyl)-3-{{[(3,4-dimethoxyphenyl)methyl]carbonyl}amino}propanoic acid ethyl ester

Base Information

Chemical Name:2-(3,4-dimethoxyphenyl)-3-{{[(3,4-dimethoxyphenyl)methyl]carbonyl}amino}propanoic acid ethyl ester
CAS No.:95520-62-0
Molecular Formula:C₂₃H₂₉NO₇
Molecular Weight:431.486
Hs Code.:

Synonyms:2-(3,4-dimethoxyphenyl)-3-{{[(3,4-dimethoxyphenyl)methyl]carbonyl}amino}propanoic acid ethyl ester

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Chemical Property of 2-(3,4-dimethoxyphenyl)-3-{{[(3,4-dimethoxyphenyl)methyl]carbonyl}amino}propanoic acid ethyl ester

Chemical Property:

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Technology Process of 2-(3,4-dimethoxyphenyl)-3-{{[(3,4-dimethoxyphenyl)methyl]carbonyl}amino}propanoic acid ethyl ester

There total 3 articles about 2-(3,4-dimethoxyphenyl)-3-{{[(3,4-dimethoxyphenyl)methyl]carbonyl}amino}propanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 3,4-dimethoxyphenyl acetic acid chloride

: 16226-24-7
α-aminomethyl-(3,4-dimethoxy)benzene acetic acid ethyl ester hydrochloride

: 95520-62-0
2-(3,4-dimethoxyphenyl)-3-{{[(3,4-dimethoxyphenyl)methyl]carbonyl}amino}propanoic acid ethyl ester

Guidance literature:: With hydrogenchloride; sodium hydroxide; thionyl chloride; In dichloromethane; water; toluene;

Reference yield:

: 93-17-4
3,4-dimethoxyphenylacetonitrile

: 95520-62-0
2-(3,4-dimethoxyphenyl)-3-{{[(3,4-dimethoxyphenyl)methyl]carbonyl}amino}propanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium / ethanol; toluene

1.2: 80 °C

2.1: hydrogenchloride; palladium on activated charcoal; hydrogen / ethanol / 2585.81 Torr

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane

With hydrogenchloride; palladium on activated charcoal; hydrogen; sodium; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In ethanol; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2011.09.009

Reference yield:

: 36848-69-8
ethyl 2-cyano-2-(3,4-dimethoxyphenyl)acetate

: 95520-62-0
2-(3,4-dimethoxyphenyl)-3-{{[(3,4-dimethoxyphenyl)methyl]carbonyl}amino}propanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; palladium on activated charcoal; hydrogen / ethanol / 2585.81 Torr

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane

With hydrogenchloride; palladium on activated charcoal; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.09.009