3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole

Base Information

• Chemical Name: 3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole
• CAS No.: 1174231-65-2
• Molecular Formula: C₁₅H₂₁ClN₂OSSi
• Molecular Weight: 340.949

Synonyms:3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole

Chemical Property of 3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole

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Technology Process of 3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole

There total 1 articles about 3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

5-phenylthio-1-<2-(trimethylsilyl)ethoxy>methyl-1H-pyrazole (133560-59-5) → 3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole (1174231-65-2)

Guidance literature:

5-phenylthio-1-<2-(trimethylsilyl)ethoxy>methyl-1H-pyrazole; With 2,2,6,6-tetramethyl-piperidyl-MgCl*LiCl; In tetrahydrofuran; at -15 ℃; for 10h; Inert atmosphere;

With 1,1,2-Trichloro-1,2,2-trifluoroethane; In tetrahydrofuran; at -15 - 25 ℃; Inert atmosphere;

DOI:10.1021/ol901208d

Reference yield: 71.0%

3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole (1174231-65-2) + benzaldehyde (100-52-7) → (3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazol-4-yl)(phenyl)methanol (1174231-72-1)

Guidance literature:

3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole; With TMP₂Mg*2LiCl; In tetrahydrofuran; at -20 ℃; for 4h; Inert atmosphere;

benzaldehyde; In tetrahydrofuran; at -20 - 25 ℃; Inert atmosphere;

DOI:10.1021/ol901208d

Reference yield: 65.0%

3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole (1174231-65-2) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 3-chloro-5-phenylsulfanyl-1-(2-trimethylsilanyl-ethoxymethyl)-1H-pyrazole-4-carbaldehyde (1174231-73-2)

Guidance literature:

3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole; With TMP₂Mg*2LiCl; In tetrahydrofuran; at -20 ℃; for 4h; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; at -20 - 25 ℃; Inert atmosphere;

DOI:10.1021/ol901208d

upstream raw materials:

5-phenylthio-1-<2-(trimethylsilyl)ethoxy>methyl-1H-pyrazole

Downstream raw materials:

(3-chloro-5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazol-4-yl)(phenyl)methanol

3-chloro-5-phenylsulfanyl-1-(2-trimethylsilanyl-ethoxymethyl)-1H-pyrazole-4-carbaldehyde

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