(4-(3-((tert-butyldiphenylsilyl)oxy)propoxy)pyridine-2,6-diyl)dimethanol

Base Information

Chemical Name:(4-(3-((tert-butyldiphenylsilyl)oxy)propoxy)pyridine-2,6-diyl)dimethanol
CAS No.:1450841-35-6
Molecular Formula:C₂₆H₃₃NO₄Si
Molecular Weight:451.638
Hs Code.:

Synonyms:(4-(3-((tert-butyldiphenylsilyl)oxy)propoxy)pyridine-2,6-diyl)dimethanol

Suppliers and Price of (4-(3-((tert-butyldiphenylsilyl)oxy)propoxy)pyridine-2,6-diyl)dimethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-(3-((tert-butyldiphenylsilyl)oxy)propoxy)pyridine-2,6-diyl)dimethanol

Chemical Property:

Purity/Quality:

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Technology Process of (4-(3-((tert-butyldiphenylsilyl)oxy)propoxy)pyridine-2,6-diyl)dimethanol

There total 3 articles about (4-(3-((tert-butyldiphenylsilyl)oxy)propoxy)pyridine-2,6-diyl)dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1450841-34-5
dimethyl 4-(3-((tert-butyldiphenylsilyl)oxy)propoxy)pyridine-2,6-dicarboxylate

: 1450841-35-6
(4-(3-((tert-butyldiphenylsilyl)oxy)propoxy)pyridine-2,6-diyl)dimethanol

Guidance literature:: With lithium borohydride; In tetrahydrofuran; methanol; at 0 - 50 ℃;
DOI:10.1039/c3cc44354j

Reference yield:

: 19872-91-4
dimethyl 4-hydroxypyridine-2,6-dicarboxylate

: 1450841-35-6
(4-(3-((tert-butyldiphenylsilyl)oxy)propoxy)pyridine-2,6-diyl)dimethanol

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2: lithium borohydride / tetrahydrofuran; methanol / 0 - 50 °C

With lithium borohydride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1039/c3cc44354j

Reference yield:

: chelidamic acid

: 1450841-35-6
(4-(3-((tert-butyldiphenylsilyl)oxy)propoxy)pyridine-2,6-diyl)dimethanol

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 24 h / 50 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

3: lithium borohydride / tetrahydrofuran; methanol / 0 - 50 °C

With lithium borohydride; thionyl chloride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1039/c3cc44354j