tert-butyl (1-(4-(5-hydrazono-3-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate

Base Information

Chemical Name:tert-butyl (1-(4-(5-hydrazono-3-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate
CAS No.:1313440-22-0
Molecular Formula:C₂₉H₃₃N₅O₂
Molecular Weight:483.613
Hs Code.:

Synonyms:tert-butyl (1-(4-(5-hydrazono-3-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate

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Chemical Property of tert-butyl (1-(4-(5-hydrazono-3-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate

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Technology Process of tert-butyl (1-(4-(5-hydrazono-3-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate

There total 4 articles about tert-butyl (1-(4-(5-hydrazono-3-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313440-19-5
tert-butyl (1-(4-(3-phenyl-5-thioxo-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate

: 1313440-22-0
tert-butyl (1-(4-(5-hydrazono-3-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate

Guidance literature:: tert-butyl (1-(4-(3-phenyl-5-thioxo-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate; With mercury(II) diacetate; hydrazine hydrate; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

In toluene; for 3h; Reflux;

Reference yield:

: 1032349-98-6
tert-butyl 1-(4-(2-phenylacetyl)phenyl)cyclobutylcarbamate

: 1313440-22-0
tert-butyl (1-(4-(5-hydrazono-3-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 18 h / 80 °C / Inert atmosphere

2.1: ammonium acetate; acetic acid / 2 h / 100 °C / Inert atmosphere; Molecular sieve

3.1: Lawessons reagent / toluene / 2 h / Inert atmosphere; Reflux

4.1: mercury(II) diacetate; hydrazine hydrate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

4.2: 3 h / Reflux

With Lawessons reagent; mercury(II) diacetate; ammonium acetate; hydrazine hydrate; acetic acid; In tetrahydrofuran; toluene;

Reference yield:

: 1247897-74-0
tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate

: 1313440-22-0
tert-butyl (1-(4-(5-hydrazono-3-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium acetate; acetic acid / 2 h / 100 °C / Inert atmosphere; Molecular sieve

2.1: Lawessons reagent / toluene / 2 h / Inert atmosphere; Reflux

3.1: mercury(II) diacetate; hydrazine hydrate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3.2: 3 h / Reflux

With Lawessons reagent; mercury(II) diacetate; ammonium acetate; hydrazine hydrate; acetic acid; In tetrahydrofuran; toluene;