anti-11-chlorobicyclo<4.4.1>undeca-1,3-dien-6-ol

Base Information

• Chemical Name: anti-11-chlorobicyclo<4.4.1>undeca-1,3-dien-6-ol
• CAS No.: 83692-67-5
• Molecular Formula: C₁₁H₁₅ClO
• Molecular Weight: 198.692

Synonyms:anti-11-chlorobicyclo<4.4.1>undeca-1,3-dien-6-ol

Chemical Property of anti-11-chlorobicyclo<4.4.1>undeca-1,3-dien-6-ol

Chemical Property:

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SDS file from LookChem

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Technology Process of anti-11-chlorobicyclo<4.4.1>undeca-1,3-dien-6-ol

There total 4 articles about anti-11-chlorobicyclo<4.4.1>undeca-1,3-dien-6-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

11-bromo-11-chloro<4.4.1>propell-3-ene (83730-02-3) → tetralin (119-64-2) + anti-11-chlorobicyclo<4.4.1>undeca-1,3-dien-6-ol (83692-67-5) + anti-6-chloromethylenecyclodec-3-enone (83692-66-4) + anti-11-chloro-1,6-dihydroxybicyclo<4.4.1>undec-3-ene (83692-62-0,83730-04-5) + cis-bicyclo<4.4.0>dec-3-ene-1-carboxylic acid (83692-68-6,83692-69-7) + 1-Benzosuberone (826-73-3)

Guidance literature:

With silver perchlorate; In water; acetone; for 312h; Product distribution; Ambient temperature; Ag⁺-promoted hydrolysis of epimeric 11-bromo-11-chloro<4.4.1>propell-3-enes, stereochemical and kinetic aspects, effect of solvents ratio;

DOI:10.1021/ja00389a046

Reference yield:

1,2,3,4,5,8-hexahydro-naphthalene (36231-13-7) + chlorodibromomethane (124-48-1) → tetralin (119-64-2) + (11R,6S)- and (11S,6R)-11-chlorobicyclo<4.4.1>undeca-1(10),3-dien-6-ol (83692-65-3) + anti-11-chlorobicyclo<4.4.1>undeca-1,3-dien-6-ol (83692-67-5) + 1-Benzosuberone (826-73-3)

Guidance literature:

With silver perchlorate; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given; 2.) Me₂CO, H₂O, 13 days;

DOI:10.1021/ja00389a046

Reference yield:

1,2,3,4,5,8-hexahydro-naphthalene (36231-13-7) + chlorodibromomethane (124-48-1) → tetralin (119-64-2) + anti-11-chlorobicyclo<4.4.1>undeca-1,3-dien-6-ol (83692-67-5) + anti-6-chloromethylenecyclodec-3-enone (83692-66-4) + 1-Benzosuberone (826-73-3)

Guidance literature:

With silver perchlorate; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given; 2.) Me₂CO, H₂O, room temperature, 13 days;

DOI:10.1021/ja00389a046

upstream raw materials:

1,2,3,4,5,8-hexahydro-naphthalene

chlorodibromomethane

11-bromo-11-chloro<4.4.1>propell-3-ene

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