β-D-[3-O-(4-acetyloxy-3,5-dimethoxycinnamoyl)]fructofuranosyl-α-D-glucopyranoside

Base Information

Chemical Name:β-D-[3-O-(4-acetyloxy-3,5-dimethoxycinnamoyl)]fructofuranosyl-α-D-glucopyranoside
CAS No.:1610615-93-4
Molecular Formula:C₂₅H₃₄O₁₆
Molecular Weight:590.535
Hs Code.:

Synonyms:β-D-[3-O-(4-acetyloxy-3,5-dimethoxycinnamoyl)]fructofuranosyl-α-D-glucopyranoside

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Chemical Property of β-D-[3-O-(4-acetyloxy-3,5-dimethoxycinnamoyl)]fructofuranosyl-α-D-glucopyranoside

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Technology Process of β-D-[3-O-(4-acetyloxy-3,5-dimethoxycinnamoyl)]fructofuranosyl-α-D-glucopyranoside

There total 4 articles about β-D-[3-O-(4-acetyloxy-3,5-dimethoxycinnamoyl)]fructofuranosyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 4-acetyloxy-3,5-dimethoxycinnamic anhydride

: 57-50-1
Sucrose

: 1610615-93-4
β-D-[3-O-(4-acetyloxy-3,5-dimethoxycinnamoyl)]fructofuranosyl-α-D-glucopyranoside

Guidance literature:: Sucrose; With triethylamine; cobalt(II) chloride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

4-acetyloxy-3,5-dimethoxycinnamic anhydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Reagent/catalyst; Temperature; regioselective reaction; Catalytic behavior;
DOI:10.1016/j.tet.2014.04.050

Reference yield:

: 90985-68-5,113158-15-9
(E)-4-acetoxy-3,5-dimethoxycinnamic acid

: 1610615-93-4
β-D-[3-O-(4-acetyloxy-3,5-dimethoxycinnamoyl)]fructofuranosyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: bis(trichloromethyl) carbonate; triethylamine / ethyl acetate / 0.42 h / 0 - 20 °C

2.1: cobalt(II) chloride; triethylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 1 h / 20 °C

With bis(trichloromethyl) carbonate; triethylamine; cobalt(II) chloride; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2014.04.050

Reference yield:

: 53669-33-3
4-acetoxy-3,5-dimethoxybenzaldehyde

: 1610615-93-4
β-D-[3-O-(4-acetyloxy-3,5-dimethoxycinnamoyl)]fructofuranosyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine; pyridine / benzene / 3 h / Reflux

2.1: bis(trichloromethyl) carbonate; triethylamine / ethyl acetate / 0.42 h / 0 - 20 °C

3.1: cobalt(II) chloride; triethylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 1 h / 20 °C

With piperidine; pyridine; bis(trichloromethyl) carbonate; triethylamine; cobalt(II) chloride; In ethyl acetate; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tet.2014.04.050