4-<2-amino>phenyl>-4-(3-chlorophenyl)-4-hydroxy-N,N-dimethyl-1-butanamine

Base Information

Chemical Name:4-<2-amino>phenyl>-4-(3-chlorophenyl)-4-hydroxy-N,N-dimethyl-1-butanamine
CAS No.:96245-66-8
Molecular Formula:C₂₅H₂₉ClN₂O₃S
Molecular Weight:473.036
Hs Code.:

4-<2-<N-<(4-methylphenyl)sulfonyl>amino>phenyl>-4-(3-chlorophenyl)-4-hydroxy-N,N-dimethyl-1-butanamine

Synonyms:4-<2-amino>phenyl>-4-(3-chlorophenyl)-4-hydroxy-N,N-dimethyl-1-butanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-<2-amino>phenyl>-4-(3-chlorophenyl)-4-hydroxy-N,N-dimethyl-1-butanamine

Chemical Property:

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Technology Process of 4-<2-amino>phenyl>-4-(3-chlorophenyl)-4-hydroxy-N,N-dimethyl-1-butanamine

There total 6 articles about 4-<2-amino>phenyl>-4-(3-chlorophenyl)-4-hydroxy-N,N-dimethyl-1-butanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 19070-16-7
3-(N,N-dimethylamino)propylmagnesium chloride

: 96245-65-7
2-amino>-3'-chlorobenzophenone

: 96245-66-8
4-<2-amino>phenyl>-4-(3-chlorophenyl)-4-hydroxy-N,N-dimethyl-1-butanamine

Guidance literature:: In toluene; for 10h; Heating;
DOI:10.1021/jm00145a005

Reference yield:

: 96245-64-6
2-[(3-Chloro-phenyl)-imino-methyl]-phenylamine

: 96245-66-8
4-<2-amino>phenyl>-4-(3-chlorophenyl)-4-hydroxy-N,N-dimethyl-1-butanamine

Guidance literature:: Multi-step reaction with 3 steps

1: water, 25 percent H₂SO₄ / diethyl ether

2: 71 percent / pyridine / 1 h / Heating

3: 74 percent / toluene / 10 h / Heating

With sulfuric acid; water; In pyridine; diethyl ether; toluene;
DOI:10.1021/jm00145a005

Reference yield:

: 36229-42-2
(3-chlorophenyl)magnesium bromide

: 96245-66-8
4-<2-amino>phenyl>-4-(3-chlorophenyl)-4-hydroxy-N,N-dimethyl-1-butanamine

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether; toluene / 1 h / 100 °C

2: water, 25 percent H₂SO₄ / diethyl ether

3: 71 percent / pyridine / 1 h / Heating

4: 74 percent / toluene / 10 h / Heating

With sulfuric acid; water; In pyridine; diethyl ether; toluene;
DOI:10.1021/jm00145a005