nonyl 4,5-dimethoxy-2-nitrobenzylcarbamate

Base Information

• Chemical Name: nonyl 4,5-dimethoxy-2-nitrobenzylcarbamate
• CAS No.: 1380431-41-3
• Molecular Formula: C₁₉H₃₀N₂O₆
• Molecular Weight: 382.457
• Mol file: 1380431-41-3.mol

Synonyms:nonyl 4,5-dimethoxy-2-nitrobenzylcarbamate

Chemical Property of nonyl 4,5-dimethoxy-2-nitrobenzylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of nonyl 4,5-dimethoxy-2-nitrobenzylcarbamate

There total 2 articles about nonyl 4,5-dimethoxy-2-nitrobenzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

chloroformic acid n-nonyl ester (57045-82-6) + (4,5-dimethoxy-2-nitrophenyl)methanamine (123330-73-4) → nonyl 4,5-dimethoxy-2-nitrobenzylcarbamate (1380431-41-3)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1039/c1pp05308f

Reference yield:

4,5-dimethoxy-2-nitrobenzaldehyde O-acetyl oxime → nonyl 4,5-dimethoxy-2-nitrobenzylcarbamate (1380431-41-3)

Guidance literature:

Multi-step reaction with 3 steps

1: borane-THF / tetrahydrofuran / 24 h / 0 °C / Inert atmosphere; Reflux

2: potassium hydroxide / water / 3 h / -20 - 20 °C

3: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With borane-THF; triethylamine; potassium hydroxide; In tetrahydrofuran; dichloromethane; water;

DOI:10.1039/c1pp05308f

upstream raw materials:

chloroformic acid n-nonyl ester

(4,5-dimethoxy-2-nitrophenyl)methanamine