(2S)-2-[(methoxymethoxy)methyl]-1-[[(1R)-2-methoxy-1-(3-methyl-2-butenyl)-2,5-cyclohexadien-1-yl]carbonyl]pyrrolidine

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Chemical Name:(2S)-2-[(methoxymethoxy)methyl]-1-[[(1R)-2-methoxy-1-(3-methyl-2-butenyl)-2,5-cyclohexadien-1-yl]carbonyl]pyrrolidine
CAS No.:1071198-94-1
Molecular Formula:C₂₀H₃₁NO₄
Molecular Weight:349.47
Hs Code.:

Synonyms:(2S)-2-[(methoxymethoxy)methyl]-1-[[(1R)-2-methoxy-1-(3-methyl-2-butenyl)-2,5-cyclohexadien-1-yl]carbonyl]pyrrolidine

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Chemical Property of (2S)-2-[(methoxymethoxy)methyl]-1-[[(1R)-2-methoxy-1-(3-methyl-2-butenyl)-2,5-cyclohexadien-1-yl]carbonyl]pyrrolidine

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Technology Process of (2S)-2-[(methoxymethoxy)methyl]-1-[[(1R)-2-methoxy-1-(3-methyl-2-butenyl)-2,5-cyclohexadien-1-yl]carbonyl]pyrrolidine

There total 1 articles about (2S)-2-[(methoxymethoxy)methyl]-1-[[(1R)-2-methoxy-1-(3-methyl-2-butenyl)-2,5-cyclohexadien-1-yl]carbonyl]pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 102069-85-2
2-methoxy-1-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>benzene

: 870-63-3
prenyl bromide

: 1071198-94-1
(2S)-2-[(methoxymethoxy)methyl]-1-[[(1R)-2-methoxy-1-(3-methyl-2-butenyl)-2,5-cyclohexadien-1-yl]carbonyl]pyrrolidine

Guidance literature:: 2-methoxy-1-<<2(S)-<(methoxymethoxy)methyl>pyrrolidinyl>carbonyl>benzene; With ammonia; potassium; In tetrahydrofuran; tert-butyl alcohol; at -78 ℃; for 0.333333h;

prenyl bromide; In tetrahydrofuran; tert-butyl alcohol; at -78 - 25 ℃;
DOI:10.1021/jo8015743

Reference yield: 55.0%

: 67-56-1
methanol

: 1071198-94-1
(2S)-2-[(methoxymethoxy)methyl]-1-[[(1R)-2-methoxy-1-(3-methyl-2-butenyl)-2,5-cyclohexadien-1-yl]carbonyl]pyrrolidine

: 79-22-1
methyl chloroformate

: 1071198-99-6
methyl (2S)-2-[[[[(1R)-1-(3-methyl-2-butenyl)-6-oxo-2-cyclohexen-1-yl]carbonyl]oxy]methyl]-1-pyrrolidinecarboxylate

: 1071199-01-3
C₂₀H₃₁NO₆

Guidance literature:: methanol; (2S)-2-[(methoxymethoxy)methyl]-1-[[(1R)-2-methoxy-1-(3-methyl-2-butenyl)-2,5-cyclohexadien-1-yl]carbonyl]pyrrolidine; With hydrogenchloride; water; at 65 ℃; for 0.133333h; Microwave irradiation;

methyl chloroformate; With sodium hydrogencarbonate; In dichloromethane; at 0 - 25 ℃; for 3h;
DOI:10.1021/jo8015743