trans-4-benzyloxycarbonylmethyl-1-t-butyldimethylsilyloxycyclohexane

Base Information

Chemical Name:trans-4-benzyloxycarbonylmethyl-1-t-butyldimethylsilyloxycyclohexane
CAS No.:929556-43-4
Molecular Formula:C₂₁H₃₄O₃Si
Molecular Weight:362.585
Hs Code.:

Synonyms:trans-4-benzyloxycarbonylmethyl-1-t-butyldimethylsilyloxycyclohexane

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Chemical Property of trans-4-benzyloxycarbonylmethyl-1-t-butyldimethylsilyloxycyclohexane

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Technology Process of trans-4-benzyloxycarbonylmethyl-1-t-butyldimethylsilyloxycyclohexane

There total 6 articles about trans-4-benzyloxycarbonylmethyl-1-t-butyldimethylsilyloxycyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 929557-12-0
trans-4-benzyloxycarbonylmethyl-1-hydroxycyclohexane

: 18162-48-6
tert-butyldimethylsilyl chloride

: 929556-43-4
trans-4-benzyloxycarbonylmethyl-1-t-butyldimethylsilyloxycyclohexane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 - 60 ℃; for 3h;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 929556-43-4
trans-4-benzyloxycarbonylmethyl-1-t-butyldimethylsilyloxycyclohexane

Guidance literature:: Multi-step reaction with 5 steps

1.1: benzoic acid / toluene / 48 h / 20 - 95 °C

2.1: diphenyl sulfide; hydrogen / palladium 10% on activated carbon / methanol / 40 h / 20 °C

3.1: water; toluene-4-sulfonic acid / acetone / 10 h / 55 °C

4.1: sodium tetrahydroborate / methanol / 2 h / 0 °C

4.2: pH 4

5.1: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 - 60 °C

With 1H-imidazole; sodium tetrahydroborate; diphenyl sulfide; water; hydrogen; toluene-4-sulfonic acid; benzoic acid; palladium 10% on activated carbon; In methanol; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 929557-09-5
benzyl 2-(1,4-dioxaspiro[4,5]decan-8-ylidene)acetate

: 929556-43-4
trans-4-benzyloxycarbonylmethyl-1-t-butyldimethylsilyloxycyclohexane

Guidance literature:: Multi-step reaction with 4 steps

1.1: diphenyl sulfide; hydrogen / palladium 10% on activated carbon / methanol / 40 h / 20 °C

2.1: water; toluene-4-sulfonic acid / acetone / 10 h / 55 °C

3.1: sodium tetrahydroborate / methanol / 2 h / 0 °C

3.2: pH 4

4.1: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 - 60 °C

With 1H-imidazole; sodium tetrahydroborate; diphenyl sulfide; water; hydrogen; toluene-4-sulfonic acid; palladium 10% on activated carbon; In methanol; N,N-dimethyl-formamide; acetone;