2-(3,5-bis(dodecyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3,5-bis(dodecyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1589027-98-4
Molecular Formula:C₃₆H₆₅BO₄
Molecular Weight:572.721
Hs Code.:

Synonyms:2-(3,5-bis(dodecyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-(3,5-bis(dodecyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(3,5-bis(dodecyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 5 articles about 2-(3,5-bis(dodecyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1589027-95-1
C₃₀H₅₃IO₂

: 73183-34-3
bis(pinacol)diborane

: 1589027-98-4
2-(3,5-bis(dodecyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In N,N-dimethyl-formamide; at 60 ℃;
DOI:10.1039/c3ra47633b

Reference yield: 51.0%

: 1416794-30-3
1-bromo-3,5-bis(dodecyloxy)benzene

: 73183-34-3
bis(pinacol)diborane

: 1589027-98-4
2-(3,5-bis(dodecyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In tetrahydrofuran; for 5h; Reflux; Inert atmosphere;
DOI:10.1039/c8cc01594e

Reference yield:

: 143-15-7
1-dodecylbromide

: 1589027-98-4
2-(3,5-bis(dodecyloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetone / Reflux

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 60 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; acetone; 2: |Miyaura Borylation Reaction;
DOI:10.1039/c3ra47633b