(S)-2-(2,6-Dichloro-phenoxy)-propionimidic acid ethyl ester; hydrochloride

Base Information

Chemical Name:(S)-2-(2,6-Dichloro-phenoxy)-propionimidic acid ethyl ester; hydrochloride
CAS No.:101934-15-0
Molecular Formula:C₁₁H₁₃Cl₂NO₂*ClH
Molecular Weight:298.597
Hs Code.:

Synonyms:(S)-2-(2,6-Dichloro-phenoxy)-propionimidic acid ethyl ester; hydrochloride

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Chemical Property of (S)-2-(2,6-Dichloro-phenoxy)-propionimidic acid ethyl ester; hydrochloride

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Technology Process of (S)-2-(2,6-Dichloro-phenoxy)-propionimidic acid ethyl ester; hydrochloride

There total 5 articles about (S)-2-(2,6-Dichloro-phenoxy)-propionimidic acid ethyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-17-5
ethanol

: 87789-43-3
(+)-2-(2,6-dichlorophenoxy)propionitrile

: 101934-15-0
(S)-2-(2,6-Dichloro-phenoxy)-propionimidic acid ethyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In chloroform; at 0 ℃; for 36h;
DOI:10.1021/jm00157a011

Reference yield:

: 87-65-0
2,6-Dichlorophenol

: 101934-15-0
(S)-2-(2,6-Dichloro-phenoxy)-propionimidic acid ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) potassium methoxide / 1.) 2-butanone, 40 deg C, 1 h, 2.) 2-butanone, 70 deg C, 20 h

2: 73 percent / 33percent aq. NH₃ / ethanol / 48 h / Ambient temperature

3: 84 percent / TiCl₄, N-methylmorpholine / CHCl₃; tetrahydrofuran / 12 h / Ambient temperature

4: HCl gas / CHCl₃ / 36 h / 0 °C

With 4-methyl-morpholine; hydrogenchloride; ammonium hydroxide; potassium methanolate; titanium tetrachloride; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1021/jm00157a011

Reference yield:

: 1206899-43-5
(-)-2-(2,6-dichlorophenoxy)propionamide

: 101934-15-0
(S)-2-(2,6-Dichloro-phenoxy)-propionimidic acid ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / TiCl₄, N-methylmorpholine / CHCl₃; tetrahydrofuran / 12 h / Ambient temperature

2: HCl gas / CHCl₃ / 36 h / 0 °C

With 4-methyl-morpholine; hydrogenchloride; titanium tetrachloride; In tetrahydrofuran; chloroform;
DOI:10.1021/jm00157a011