5-O-benzoyl-4-C-hydroxymethyl-2,3-O-isopropylidene-1-O-methyl-β-D-ribofuranose

Base Information

Chemical Name:5-O-benzoyl-4-C-hydroxymethyl-2,3-O-isopropylidene-1-O-methyl-β-D-ribofuranose
CAS No.:327614-69-7
Molecular Formula:C₁₇H₂₂O₇
Molecular Weight:338.357
Hs Code.:

Synonyms:5-O-benzoyl-4-C-hydroxymethyl-2,3-O-isopropylidene-1-O-methyl-β-D-ribofuranose

Suppliers and Price of 5-O-benzoyl-4-C-hydroxymethyl-2,3-O-isopropylidene-1-O-methyl-β-D-ribofuranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 5-O-benzoyl-4-C-hydroxymethyl-2,3-O-isopropylidene-1-O-methyl-β-D-ribofuranose

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

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Technology Process of 5-O-benzoyl-4-C-hydroxymethyl-2,3-O-isopropylidene-1-O-methyl-β-D-ribofuranose

There total 7 articles about 5-O-benzoyl-4-C-hydroxymethyl-2,3-O-isopropylidene-1-O-methyl-β-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₃₁H₃₆O₈

: 98-88-4
benzoyl chloride

: 327614-69-7
5-O-benzoyl-4-C-hydroxymethyl-2,3-O-isopropylidene-1-O-methyl-β-D-ribofuranose

Guidance literature:: C₃₁H₃₆O₈; benzoyl chloride; With pyridine; at 20 ℃; for 13h; Inert atmosphere;

With acetic acid; at 20 ℃; for 3h;

Reference yield:

: Benzoic acid (3aS,4R,6R,6aR)-4-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

: 327614-69-7
5-O-benzoyl-4-C-hydroxymethyl-2,3-O-isopropylidene-1-O-methyl-β-D-ribofuranose

Guidance literature:: With acetic acid; at 20 ℃; for 2h;
DOI:10.1016/S0968-0896(00)00221-2

Reference yield:

: 33985-40-9
(3aR,4S,6R,6aR)-tetrahydro-6-methoxy-2,2-dimethylfuro-[3,4-d][1,3]dioxole-4-carbaldehyde

: 327614-69-7
5-O-benzoyl-4-C-hydroxymethyl-2,3-O-isopropylidene-1-O-methyl-β-D-ribofuranose

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / aq. NaOH / dioxane / 20 °C

2: 77 percent / pyridine / 20 °C

3: pyridine / 20 °C

4: aq. AcOH / 2 h / 20 °C

With sodium hydroxide; acetic acid; In 1,4-dioxane; pyridine;
DOI:10.1016/S0968-0896(00)00221-2