4-nitrophenyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Base Information

Chemical Name:4-nitrophenyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside
CAS No.:142329-94-0
Molecular Formula:C₁₇H₂₂N₂O₈
Molecular Weight:382.37
Hs Code.:

Synonyms:4-nitrophenyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Suppliers and Price of 4-nitrophenyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-nitrophenyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-nitrophenyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

There total 4 articles about 4-nitrophenyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77-76-9
2,2-dimethoxy-propane

: 3459-18-5,50645-66-4
4-nitrophenyl N-acetyl-β-D-glucosaminide

: 142329-94-0
4-nitrophenyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.carres.2007.05.023

Reference yield:

: 13089-27-5,13089-23-1
p-nitrophenyl 2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranoside

: 142329-94-0
4-nitrophenyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / NaOCH₃; MeOH / CHCl₃

2: 4-TsOH*H₂O / dimethylformamide / 20 °C

With methanol; sodium methylate; toluene-4-sulfonic acid; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2007.05.023

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 142329-94-0
4-nitrophenyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 20 °C

1.2: 44 percent / K₂CO₃ / acetone / 55 °C

2.1: 97 percent / NaOCH₃; MeOH / CHCl₃

3.1: 4-TsOH*H₂O / dimethylformamide / 20 °C

With methanol; sodium methylate; toluene-4-sulfonic acid; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2007.05.023