<5,10,15,20-tetrakis(2,6-dimethylphenyl)porphinato>zinc(II)

Base Information

Chemical Name:<5,10,15,20-tetrakis(2,6-dimethylphenyl)porphinato>zinc(II)
CAS No.:91947-22-7
Molecular Formula:C₅₂H₄₄N₄Zn
Molecular Weight:790.338
Hs Code.:

Synonyms:<5,10,15,20-tetrakis(2,6-dimethylphenyl)porphinato>zinc(II)

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Chemical Property of <5,10,15,20-tetrakis(2,6-dimethylphenyl)porphinato>zinc(II)

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Technology Process of <5,10,15,20-tetrakis(2,6-dimethylphenyl)porphinato>zinc(II)

There total 2 articles about <5,10,15,20-tetrakis(2,6-dimethylphenyl)porphinato>zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 557-34-6
zinc diacetate

: 104292-54-8
5,10,15,20-tetrakis(2,6-dimethylphenyl)porphyrin

: 91947-22-7
(5,10,15,20-tetrakis(2,6-dimethylphenyl)porphinato)zinc(II)

Guidance literature:: In tetrahydrofuran; Reflux; Inert atmosphere;
DOI:10.1021/jacs.0c07781

Reference yield: 4.6%

: 109-97-7,30604-81-0
pyrrole

: 5970-45-6
zinc(II) acetate dihydrate

: 1123-56-4
2,6-dimethylbenzaldehyde

: 91947-22-7
(5,10,15,20-tetrakis(2,6-dimethylphenyl)porphinato)zinc(II)

: C₂₀H₁₀N₄((CH₃)2C₆H₃)4Zn

Guidance literature:: In pyridine; ArCHO, pyrrole, Zn-acetate and pyridine were sealed in a heavy-walled glass reaction bomb and heated in an oven at 185°C for 65 h; mixt. washed with acetone, washes were combined, dild. with acetone, placed in the freezer for 8 d, ppt. was filtered, washed with cold acetone; sepn. of crude product (C6H6, addn. of O2C6Cl2(CN)2, reflux for 3 d, column chromy./C6H6-CH2Cl2, evapn.);
DOI:10.1021/ja00275a033