(S)-N-((S)-1-(3-chloro-2,6-difluorophenyl)but-3-en-1-yl)-2-methylpropane-2-sulfmamide

Base Information

Chemical Name:(S)-N-((S)-1-(3-chloro-2,6-difluorophenyl)but-3-en-1-yl)-2-methylpropane-2-sulfmamide
CAS No.:1422510-33-5
Molecular Formula:C₁₄H₁₈ClF₂NOS
Molecular Weight:321.819
Hs Code.:

Synonyms:(S)-N-((S)-1-(3-chloro-2,6-difluorophenyl)but-3-en-1-yl)-2-methylpropane-2-sulfmamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-((S)-1-(3-chloro-2,6-difluorophenyl)but-3-en-1-yl)-2-methylpropane-2-sulfmamide

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Technology Process of (S)-N-((S)-1-(3-chloro-2,6-difluorophenyl)but-3-en-1-yl)-2-methylpropane-2-sulfmamide

There total 2 articles about (S)-N-((S)-1-(3-chloro-2,6-difluorophenyl)but-3-en-1-yl)-2-methylpropane-2-sulfmamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422510-32-4
(S,E)-N-(3-chloro-2,6-difluorobenzylidene)-2-methylpropane-2-sulfinamide

: 1730-25-2
allylmagnesium bromide

: 1422510-33-5
(S)-N-((S)-1-(3-chloro-2,6-difluorophenyl)but-3-en-1-yl)-2-methylpropane-2-sulfmamide

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 1.5h;

Reference yield:

: 190011-87-1
1-(3-chloro-2,6-difluoro-phenyl)-carboxaldehyde

: 1422510-33-5
(S)-N-((S)-1-(3-chloro-2,6-difluorophenyl)but-3-en-1-yl)-2-methylpropane-2-sulfmamide

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / dichloromethane / 20 °C

2: tetrahydrofuran; diethyl ether / 1.5 h / -78 - 20 °C

With caesium carbonate; In tetrahydrofuran; diethyl ether; dichloromethane;