Technology Process of 3-benzyl-4-methylpentanoic acid
There total 18 articles about 3-benzyl-4-methylpentanoic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 62 percent / potassium chromate, H2SO4
2: 72 percent / acetic acid, ammonium acetate / benzene / 25 h / Heating
3: 95 percent / H2 / 5percent Pd/C / aq. ethanol / 13 h / 760 Torr / Ambient temperature
4: 1.) acetic acid, cc. H2SO4; 2.) acetic acid, cc. H2SO4 / 1.) water, 20 h, reflux; 2.) water, 6 h, reflux
With
ammonium acetate; potassium chromate; sulfuric acid; hydrogen; acetic acid;
palladium on activated charcoal;
In
ethanol; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 72 percent / acetic acid, ammonium acetate / benzene / 25 h / Heating
2: 95 percent / H2 / 5percent Pd/C / aq. ethanol / 13 h / 760 Torr / Ambient temperature
3: 1.) acetic acid, cc. H2SO4; 2.) acetic acid, cc. H2SO4 / 1.) water, 20 h, reflux; 2.) water, 6 h, reflux
With
ammonium acetate; sulfuric acid; hydrogen; acetic acid;
palladium on activated charcoal;
In
ethanol; benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 95 percent / H2 / 5percent Pd/C / aq. ethanol / 13 h / 760 Torr / Ambient temperature
2: 1.) acetic acid, cc. H2SO4; 2.) acetic acid, cc. H2SO4 / 1.) water, 20 h, reflux; 2.) water, 6 h, reflux
With
sulfuric acid; hydrogen; acetic acid;
palladium on activated charcoal;
In
ethanol;