1-((((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-(2,6)-diisopropylphenyl)imidazolium iodide

Base Information

Chemical Name:1-((((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-(2,6)-diisopropylphenyl)imidazolium iodide
CAS No.:369657-24-9
Molecular Formula:C₃₀H₄₂N₃O*I
Molecular Weight:587.587
Hs Code.:

Synonyms:1-((((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-(2,6)-diisopropylphenyl)imidazolium iodide

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Chemical Property of 1-((((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-(2,6)-diisopropylphenyl)imidazolium iodide

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Technology Process of 1-((((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-(2,6)-diisopropylphenyl)imidazolium iodide

There total 9 articles about 1-((((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-(2,6)-diisopropylphenyl)imidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 25364-47-0
1-(2,6-diisopropylphenyl)-1H-imidazole

: 369657-19-2
(S)-2-(adamantan-1-yl)-4-(2-iodoethyl)-4,5-dihydrooxazole

: 369657-24-9
1-((((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-(2,6)-diisopropylphenyl)imidazolium iodide

Guidance literature:: In N,N-dimethyl-formamide; at 80 ℃; for 10h;
DOI:10.1021/ja016011p

Reference yield:

: 369657-20-5
(S)-2-(1-adamantyl)-4-[2-(p-toluenesulfonyl)ethyl]oxazoline

: 369657-24-9
1-((((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-(2,6)-diisopropylphenyl)imidazolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / KI / acetone / 4 h / 56 °C

2: dimethylformamide / 12 h / 80 °C

With potassium iodide; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja028142b

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 369657-24-9
1-((((S)-4',5'-dihydro-2'-(1-adamantyl)-4'-oxazolyl)ethyl)-3-(2,6)-diisopropylphenyl)imidazolium iodide

Guidance literature:: Multi-step reaction with 5 steps

1: H₂O / 0.5 h

2: ethanol / Heating

3: aq. HCl / 0.5 h / 100 °C

4: 20percent aq. HNO₃ / 0.08 h / 100 °C

5: dimethylformamide / 12 h / 80 °C

With hydrogenchloride; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ja028142b