di(-)menthyl 1-methylbutylidenemalonate

Base Information

Chemical Name:di(-)menthyl 1-methylbutylidenemalonate
CAS No.:73651-43-1
Molecular Formula:C₂₈H₄₈O₄
Molecular Weight:448.687
Hs Code.:

Synonyms:di(-)menthyl 1-methylbutylidenemalonate

Suppliers and Price of di(-)menthyl 1-methylbutylidenemalonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(-)menthyl 1-methylbutylidenemalonate

Chemical Property:

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Technology Process of di(-)menthyl 1-methylbutylidenemalonate

There total 3 articles about di(-)menthyl 1-methylbutylidenemalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18795-91-0
2-(1-methylbutylidene)malonic acid diethyl ester

: 73651-43-1
di(-)menthyl 1-methylbutylidenemalonate

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / KOH / aq. ethanol / 4 h / Heating

2: 1) SOCl₂ / 1) 1,5h / reflux 2) 100-130 deg C / 4h

With potassium hydroxide; thionyl chloride; In ethanol;
DOI:10.1021/jo01302a004

Reference yield:

: 107-87-9
2-Pentanone

: 73651-43-1
di(-)menthyl 1-methylbutylidenemalonate

Guidance literature:: Multi-step reaction with 3 steps

2: 77 percent / KOH / aq. ethanol / 4 h / Heating

3: 1) SOCl₂ / 1) 1,5h / reflux 2) 100-130 deg C / 4h

With potassium hydroxide; thionyl chloride; In ethanol;
DOI:10.1021/jo01302a004