1-azo-4-azonium-bicyclo[2.2.2]octane tris(2,2',2''-perfluorobiphenyl)borate

Base Information

Chemical Name:1-azo-4-azonium-bicyclo[2.2.2]octane tris(2,2',2''-perfluorobiphenyl)borate
CAS No.:1391927-71-1
Molecular Formula:C₆H₁₂N₂*C₃₆HBF₂₇*H
Molecular Weight:1070.35
Hs Code.:

Synonyms:1-azo-4-azonium-bicyclo[2.2.2]octane tris(2,2',2''-perfluorobiphenyl)borate

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Chemical Property of 1-azo-4-azonium-bicyclo[2.2.2]octane tris(2,2',2''-perfluorobiphenyl)borate

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Technology Process of 1-azo-4-azonium-bicyclo[2.2.2]octane tris(2,2',2''-perfluorobiphenyl)borate

There total 2 articles about 1-azo-4-azonium-bicyclo[2.2.2]octane tris(2,2',2''-perfluorobiphenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1391927-67-5
tris(2,2',2''-perfluorobiphenyl)borane - 1,4-diazobicyclo[2.2.2]octane

: 1391927-71-1
1-azo-4-azonium-bicyclo[2.2.2]octane tris(2,2',2''-perfluorobiphenyl)borate

Guidance literature:: With hydrogen; In d8-toluene; at 20 ℃; for 48h; under 760.051 Torr;
DOI:10.1039/c2dt30334e

Reference yield:

: 1391927-67-5
tris(2,2',2''-perfluorobiphenyl)borane - 1,4-diazobicyclo[2.2.2]octane

: 1333-74-0
hydrogen

: 1391927-71-1
1-azo-4-azonium-bicyclo[2.2.2]octane tris(2,2',2''-perfluorobiphenyl)borate

Guidance literature:: In ⁽²⁾H₈-toluene; (N2, Schlenk or glovebox) an NMR tube with a soln. in toluene-d8 was backfilled with H2 (1 atm), sealed, heated to 90°C for 3 days; not sepd., detected by NMR spectra;
DOI:10.1039/c2dt30334e