Technology Process of C28H36O2Si
There total 4 articles about C28H36O2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluorormethanesulfonic acid;
In
dichloromethane; cyclohexane;
at 0 ℃;
for 16h;
DOI:10.1039/c3ob27508f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / nujol; tetrahydrofuran / 16.5 h / 0 - 20 °C
1.2: 3 h / 0 - 20 °C
2.1: Amano lipase / di-isopropyl ether / 12 h / 20 °C / Enzymatic reaction
3.1: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 16 h / 0 °C
With
trifluorormethanesulfonic acid; Amano lipase; sodium hydride;
In
tetrahydrofuran; nujol; dichloromethane; di-isopropyl ether; cyclohexane;
DOI:10.1039/c3ob27508f
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 16.5 h / -10 - 20 °C
2.1: sodium hydride / nujol; tetrahydrofuran / 16.5 h / 0 - 20 °C
2.2: 3 h / 0 - 20 °C
3.1: Amano lipase / di-isopropyl ether / 12 h / 20 °C / Enzymatic reaction
4.1: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 16 h / 0 °C
With
lithium aluminium tetrahydride; trifluorormethanesulfonic acid; Amano lipase; sodium hydride;
In
tetrahydrofuran; nujol; dichloromethane; di-isopropyl ether; cyclohexane;
DOI:10.1039/c3ob27508f