C₂₉H₃₅N₇O₇

Base Information

• Chemical Name: C₂₉H₃₅N₇O₇
• CAS No.: 1293397-32-6
• Molecular Formula: C₂₉H₃₅N₇O₇
• Molecular Weight: 593.64
• Mol file: 1293397-32-6.mol

Synonyms:C₂₉H₃₅N₇O₇

Chemical Property of C₂₉H₃₅N₇O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₅N₇O₇

There total 2 articles about C₂₉H₃₅N₇O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethanol (86770-67-4) + 4-benzoyl-2-(R)-methyl-1-[(4-nitro-7-oxido-1H-pyrrolo[2,3-b]pyridin-3-yl)oxoacetyl]piperazine (357262-96-5) → C29H35N7O7 (1293397-32-6)

Guidance literature:

2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethanol; With sodium hydride; In 1,2-dimethoxyethane; for 2h; Inert atmosphere;

4-benzoyl-2-(R)-methyl-1-[(4-nitro-7-oxido-1H-pyrrolo[2,3-b]pyridin-3-yl)oxoacetyl]piperazine; In 1,2-dimethoxyethane; at 50 ℃; for 3h; Inert atmosphere;

With phosphorus trichloride; In ethyl acetate; at 20 ℃; for 2.5h; Inert atmosphere;

DOI:10.1021/ml400097z

Reference yield:

→ C29H35N7O7 (1293397-32-6)

Guidance literature:

Reference yield: 57.0%

C29H35N7O7 (1293397-32-6) + 1-(4-(2,5,8,11,14-pentaoxaheptadec-16-yn-1-yl)benzoyl)azetidin-2-one (1430096-70-0) → C51H64N8O14 (1430096-72-2)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; 3-[4-[[bis[[1-(3-hydroxypropyl)triazol-4-yl]methyl]amino]methyl]triazol-1-yl]propan-1-ol; In water; tert-butyl alcohol; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/ml400097z

upstream raw materials:

2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethanol

4-benzoyl-2-(R)-methyl-1-[(4-nitro-7-oxido-1H-pyrrolo[2,3-b]pyridin-3-yl)oxoacetyl]piperazine

Downstream raw materials:

C₅₁H₆₄N₈O₁₄

Refernces

• 1、 -. "BIFUNCTIONAL MOLECULES WITH ANTIBODY-RECRUITING AND ENTRY INHIBITORY ACTIVITY AGAINST THE HUMAN IMMUNODEFICIENCY VIRUS". Page/Page column 33-34. . Retrieved 2012/11/07.