2-(N-benzenecarbonylamino)-6-(N-benzyloxycarbonylamino)-N-benzylhexanamide

Base Information

Chemical Name:2-(N-benzenecarbonylamino)-6-(N-benzyloxycarbonylamino)-N-benzylhexanamide
CAS No.:1456905-53-5
Molecular Formula:C₂₈H₃₁N₃O₄
Molecular Weight:473.572
Hs Code.:

Synonyms:2-(N-benzenecarbonylamino)-6-(N-benzyloxycarbonylamino)-N-benzylhexanamide

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Chemical Property of 2-(N-benzenecarbonylamino)-6-(N-benzyloxycarbonylamino)-N-benzylhexanamide

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Technology Process of 2-(N-benzenecarbonylamino)-6-(N-benzyloxycarbonylamino)-N-benzylhexanamide

There total 4 articles about 2-(N-benzenecarbonylamino)-6-(N-benzyloxycarbonylamino)-N-benzylhexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 118865-76-2
2-amino-N-benzyl-6-{(benzyloxycarbonyl)amino}hexanamide hydrochloride

: 65-85-0,8013-63-6
benzoic acid

: 1456905-53-5
2-(N-benzenecarbonylamino)-6-(N-benzyloxycarbonylamino)-N-benzylhexanamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 19h;
DOI:10.1002/anie.201303999

Reference yield:

: 2389-45-9
Boc-Lys(Z)-OH

: 1456905-53-5
2-(N-benzenecarbonylamino)-6-(N-benzyloxycarbonylamino)-N-benzylhexanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 13.5 h / 20 °C

2: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C / Cooling with ice

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 19 h / 20 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201303999

Reference yield:

: 123441-84-9
6-(N-benzyloxycarbonyl)amino-2-(N-tert-butoxycarbonylamino)-N-benzylhexanamide

: 1456905-53-5
2-(N-benzenecarbonylamino)-6-(N-benzyloxycarbonylamino)-N-benzylhexanamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C / Cooling with ice

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 19 h / 20 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201303999