benzo-3-(2,4,6-tri-tert-butylphenyl)-1,3,2-dioxaphospholane

Base Information Edit

Chemical Name:benzo-3-(2,4,6-tri-tert-butylphenyl)-1,3,2-dioxaphospholane
CAS No.:151984-82-6
Molecular Formula:C₂₄H₃₃O₂P
Molecular Weight:384.499
Hs Code.:
Mol file:151984-82-6.mol

Synonyms:benzo-3-(2,4,6-tri-tert-butylphenyl)-1,3,2-dioxaphospholane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzo-3-(2,4,6-tri-tert-butylphenyl)-1,3,2-dioxaphospholane Edit

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Technology Process of benzo-3-(2,4,6-tri-tert-butylphenyl)-1,3,2-dioxaphospholane

There total 1 articles about benzo-3-(2,4,6-tri-tert-butylphenyl)-1,3,2-dioxaphospholane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.4%

: 1641-40-3
pyrocatechol phosphorochloridite

: 3975-77-7
1-bromo-2,4,6-tri-tert-butylbenzene

: 151984-82-6
benzo-3-(2,4,6-tri-tert-butylphenyl)-1,3,2-dioxaphospholane

Guidance literature:: 1-bromo-2,4,6-tri-tert-butylbenzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.166667h;

pyrocatechol phosphorochloridite; In tetrahydrofuran; hexane; at -78 - 20 ℃;

In tetrahydrofuran; hexane; for 1h; Heating;
DOI:10.1002/hc.1048