N-(5,6-dimethylpyridin-2-yl)-4,5-bis-trifluoromethylphthalamic acid methyl ester

Base Information

Chemical Name:N-(5,6-dimethylpyridin-2-yl)-4,5-bis-trifluoromethylphthalamic acid methyl ester
CAS No.:1620998-47-1
Molecular Formula:C₁₈H₁₄F₆N₂O₃
Molecular Weight:420.311
Hs Code.:

Synonyms:N-(5,6-dimethylpyridin-2-yl)-4,5-bis-trifluoromethylphthalamic acid methyl ester

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Chemical Property of N-(5,6-dimethylpyridin-2-yl)-4,5-bis-trifluoromethylphthalamic acid methyl ester

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Technology Process of N-(5,6-dimethylpyridin-2-yl)-4,5-bis-trifluoromethylphthalamic acid methyl ester

There total 2 articles about N-(5,6-dimethylpyridin-2-yl)-4,5-bis-trifluoromethylphthalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1620997-88-7
C₁₂H₈F₆O₄

: 57963-08-3
2-amino-5,6-dimethylpyridine

: 1620998-47-1
N-(5,6-dimethylpyridin-2-yl)-4,5-bis-trifluoromethylphthalamic acid methyl ester

Guidance literature:: With trimethylaluminum; In toluene; at 0 - 100 ℃;

Reference yield:

: 67193-32-2
dimethyl 4,5-diiodo-1,2-benzenedicarboxylate

: 1620998-47-1
N-(5,6-dimethylpyridin-2-yl)-4,5-bis-trifluoromethylphthalamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide / N,N-dimethyl-formamide / 18 h / 80 °C

2: trimethylaluminum / toluene / 0 - 100 °C

With copper(l) iodide; trimethylaluminum; In N,N-dimethyl-formamide; toluene;