1-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-2,4-dibenzyloxybenzene

Base Information

Chemical Name:1-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-2,4-dibenzyloxybenzene
CAS No.:251921-27-4
Molecular Formula:C₃₄H₃₆O₁₂
Molecular Weight:636.653
Hs Code.:

Synonyms:1-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-2,4-dibenzyloxybenzene

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Chemical Property of 1-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-2,4-dibenzyloxybenzene

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Technology Process of 1-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-2,4-dibenzyloxybenzene

There total 5 articles about 1-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-2,4-dibenzyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 6195-80-8
2,4-bis(benzyloxy)phenol

: 74808-10-9
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate

: 251921-27-4
1-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-2,4-dibenzyloxybenzene

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -40 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1016/j.carres.2018.06.004

Reference yield: 55.0%

: 6195-80-8
2,4-bis(benzyloxy)phenol

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 251921-27-4
1-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-2,4-dibenzyloxybenzene

Guidance literature:: With sodium hydroxide; benzyltriethylammonium bromide; In chloroform; at 60 ℃; for 13h;
DOI:10.1021/np9902237

Reference yield:

: 100-39-0
benzyl bromide

: 251921-27-4
1-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-2,4-dibenzyloxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 5 percent / dimethylformamide

2: 55 percent / sodium hydroxide; benzyltriethylammonium bromide / CHCl₃ / 13 h / 60 °C

With sodium hydroxide; benzyltriethylammonium bromide; In chloroform; N,N-dimethyl-formamide; 1: Etherification / 2: Etherification;
DOI:10.1021/np9902237