Trifluoro-methanesulfonic acid 2-(4-methylene-oct-7-enyl)-3-oxo-cyclohex-1-enyl ester

Base Information

• Chemical Name: Trifluoro-methanesulfonic acid 2-(4-methylene-oct-7-enyl)-3-oxo-cyclohex-1-enyl ester
• CAS No.: 123753-46-8
• Molecular Formula: C₁₆H₂₁F₃O₄S
• Molecular Weight: 366.402

Synonyms:Trifluoro-methanesulfonic acid 2-(4-methylene-oct-7-enyl)-3-oxo-cyclohex-1-enyl ester

Chemical Property of Trifluoro-methanesulfonic acid 2-(4-methylene-oct-7-enyl)-3-oxo-cyclohex-1-enyl ester

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Technology Process of Trifluoro-methanesulfonic acid 2-(4-methylene-oct-7-enyl)-3-oxo-cyclohex-1-enyl ester

There total 1 articles about Trifluoro-methanesulfonic acid 2-(4-methylene-oct-7-enyl)-3-oxo-cyclohex-1-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-4-butene (5162-44-7) + N,N-phenylbistrifluoromethane-sulfonimide (37595-74-7) + 4-bromopent-4-en-1-ol (64180-78-5) + (1E,4E)-1,5-Dimethoxy-hexa-1,4-diene → Trifluoro-methanesulfonic acid 2-(4-methylene-oct-7-enyl)-3-oxo-cyclohex-1-enyl ester (123753-46-8)

Guidance literature:

Multistep reaction;

DOI:10.1021/jo00286a009

Reference yield: 53.0%

Trifluoro-methanesulfonic acid 2-(4-methylene-oct-7-enyl)-3-oxo-cyclohex-1-enyl ester (123753-46-8) → 2-(4-Methylene-oct-7-enyl)-phenol (123753-51-5) + 1-But-3-enyl-1,2,3,4,6,7-hexahydro-1,4a-methano-naphthalen-5-one (123753-50-4) + C15H20O (123753-48-0)

Guidance literature:

With palladium diacetate; triethylamine; triphenylphosphine; In acetonitrile; at 70 ℃;

DOI:10.1021/jo00286a009

upstream raw materials:

1-bromo-4-butene

N,N-phenylbistrifluoromethane-sulfonimide

4-bromopent-4-en-1-ol

Downstream raw materials:

2-(4-Methylene-oct-7-enyl)-phenol

1-But-3-enyl-1,2,3,4,6,7-hexahydro-1,4a-methano-naphthalen-5-one

C₁₅H₂₀O

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