2-(bromomethyl)-2,3-dihydrobenzofuran

Base Information

• Chemical Name: 2-(bromomethyl)-2,3-dihydrobenzofuran
• CAS No.: 19997-53-6
• Molecular Formula: C9H9BrO
• Molecular Weight: 213.074
• Hs Code.: 2932999099
• Mol file: 19997-53-6.mol

Synonyms:2-Bromomethyl-2,3-dihydrobenzo[b]furan;2-Bromomethyl-2,3-dihydrobenzofuran;

Chemical Property of 2-(bromomethyl)-2,3-dihydrobenzofuran

Chemical Property:

• Vapor Pressure: 0.00697mmHg at 25°C
• Refractive Index: 1.579
• Boiling Point: 279 °C at 760 mmHg
• Flash Point: 110.4 °C
• PSA: 9.23000
• Density: 1.481 g/cm³
• LogP: 2.38500

Purity/Quality:

99% ^*data from raw suppliers

2-(bromomethyl)-2,3-dihydro-1-benzofuran ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(bromomethyl)-2,3-dihydrobenzofuran

There total 10 articles about 2-(bromomethyl)-2,3-dihydrobenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-allylanisole (3698-28-0) → carbon disulfide (75-15-0,12122-00-8) + (2,3-dihydro-2-benzofuranyl)-methyl bromide (19997-53-6)

Guidance literature:

With bromine; at 0 ℃;

Reference yield:

o-Allylphenol (1745-81-9) → carbon disulfide (75-15-0,12122-00-8) + (2,3-dihydro-2-benzofuranyl)-methyl bromide (19997-53-6)

Guidance literature:

With bromine; at 0 ℃;

Reference yield:

1-allyl-2-(benzyloxy)benzene (51496-94-7) → (2,3-dihydro-2-benzofuranyl)-methyl bromide (19997-53-6) + 1-Benzyloxy-2-(2-bromo-3-fluoro-propyl)-benzene + 2-(3'-Bromo-2'-fluoropropyl)phenylbenzyl ether

Guidance literature:

With N-Bromosuccinimide; triethylamine tris(hydrogen fluoride); In dichloromethane; Yield given. Yields of byproduct given. Title compound not separated from byproducts; 1.) 0 deg C to r.t., 2 h, 2.) r.t., 6 h;

DOI:10.1016/0022-1139(95)03290-T

upstream raw materials:

2-allylanisole

2-(2,3-dibromopropyl)phenyl acetate

2-chloromercurymethyl-2,3-dihydrobenzofuran

o-Allylphenol

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