3-Buten-2-ol, 1,1,1-trifluoro-4-phenyl-, acetate, (Z)-

Base Information

Chemical Name:3-Buten-2-ol, 1,1,1-trifluoro-4-phenyl-, acetate, (Z)-
CAS No.:128779-60-2
Molecular Formula:C₁₂H₁₁F₃O₂
Molecular Weight:244.213
Hs Code.:
DSSTox Substance ID:DTXSID401210353

Synonyms:3-Buten-2-ol, 1,1,1-trifluoro-4-phenyl-, acetate, (Z)-;DTXSID401210353;128779-60-2

Suppliers and Price of 3-Buten-2-ol, 1,1,1-trifluoro-4-phenyl-, acetate, (Z)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Buten-2-ol, 1,1,1-trifluoro-4-phenyl-, acetate, (Z)-

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:244.07111408
Heavy Atom Count:17
Complexity:278

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)OC(C=CC1=CC=CC=C1)C(F)(F)F
Isomeric SMILES:CC(=O)OC(/C=C\C1=CC=CC=C1)C(F)(F)F

Technology Process of 3-Buten-2-ol, 1,1,1-trifluoro-4-phenyl-, acetate, (Z)-

There total 3 articles about 3-Buten-2-ol, 1,1,1-trifluoro-4-phenyl-, acetate, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89524-12-9
1-phenyl-3-hydroxy-4,4,4-trifluoro-1-butyne

: 128779-60-2
(Z)-1,1,1-trifluoro-4-phenylbut-3-en-2-yl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / Lindlar catalyst / hexane / 3 h / Ambient temperature

2: pyridine / CH₂Cl₂ / 10 h / Ambient temperature

With pyridine; hydrogen; Lindlar's catalyst; In hexane; dichloromethane;
DOI:10.1016/S0022-1139(00)82938-3

Reference yield:

: 536-74-3
phenylacetylene

: 128779-60-2
(Z)-1,1,1-trifluoro-4-phenylbut-3-en-2-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / 1.) lithium diisopropyl amine / tetrahydrofuran / -50 °C / 1.) 30 min.; 2.) 2 h

2: hydrogen / Lindlar catalyst / hexane / 3 h / Ambient temperature

3: pyridine / CH₂Cl₂ / 10 h / Ambient temperature

With pyridine; hydrogen; lithium diisopropyl amide; Lindlar's catalyst; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1016/S0022-1139(00)82938-3