(2S,3R,4R,5R)-2-{(R)-1-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl}-5-octyloxy-tetrahydro-furan-3,4-diol

Base Information

Chemical Name:(2S,3R,4R,5R)-2-{(R)-1-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl}-5-octyloxy-tetrahydro-furan-3,4-diol
CAS No.:189315-18-2
Molecular Formula:C₃₄H₄₄O₇
Molecular Weight:564.719
Hs Code.:

Synonyms:(2S,3R,4R,5R)-2-{(R)-1-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl}-5-octyloxy-tetrahydro-furan-3,4-diol

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Chemical Property of (2S,3R,4R,5R)-2-{(R)-1-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl}-5-octyloxy-tetrahydro-furan-3,4-diol

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Technology Process of (2S,3R,4R,5R)-2-{(R)-1-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl}-5-octyloxy-tetrahydro-furan-3,4-diol

There total 1 articles about (2S,3R,4R,5R)-2-{(R)-1-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl}-5-octyloxy-tetrahydro-furan-3,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 166021-57-4
n-octyl β-D-galactofuranoside

: 14470-28-1
mono-4-methoxytrityl chloride

: 189315-18-2
(2S,3R,4R,5R)-2-{(R)-1-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl}-5-octyloxy-tetrahydro-furan-3,4-diol

Guidance literature:: With dmap; at 20 ℃; for 4h;
DOI:10.1016/j.carres.2006.10.001

Reference yield: 84.0%

: 100-39-0
benzyl bromide

: 189315-18-2
(2S,3R,4R,5R)-2-{(R)-1-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl}-5-octyloxy-tetrahydro-furan-3,4-diol

: (2S,3S,4R,5R)-3,4-Bis-benzyloxy-2-{(R)-1-benzyloxy-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl}-5-octyloxy-tetrahydro-furan

Guidance literature:: (2S,3R,4R,5R)-2-{(R)-1-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl}-5-octyloxy-tetrahydro-furan-3,4-diol; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

benzyl bromide; In N,N-dimethyl-formamide; at 0 ℃; for 3h;
DOI:10.1016/S0008-6215(96)00268-6

Reference yield:

: 189315-18-2
(2S,3R,4R,5R)-2-{(R)-1-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl}-5-octyloxy-tetrahydro-furan-3,4-diol

: 189315-16-0
octyl 2,3,5-tri-O-benzyl-β-D-galactofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / dimethylformamide / 0.25 h / 0 °C

1.2: 84 percent / dimethylformamide / 3 h / 0 °C

2.1: 71 percent / AcOH; H₂O / 5 h / 70 °C

With water; sodium hydride; acetic acid; In N,N-dimethyl-formamide; 1.1: Metallation / 1.2: benzylation / 2.1: detritylation;
DOI:10.1016/S0008-6215(96)00268-6