β-dimethylamino-m-hydroxypropiophenone methiodide

Base Information

Chemical Name:β-dimethylamino-m-hydroxypropiophenone methiodide
CAS No.:76106-42-8
Molecular Formula:C₁₂H₁₈NO₂*I
Molecular Weight:335.185
Hs Code.:

Synonyms:β-dimethylamino-m-hydroxypropiophenone methiodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-dimethylamino-m-hydroxypropiophenone methiodide

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Technology Process of β-dimethylamino-m-hydroxypropiophenone methiodide

There total 3 articles about β-dimethylamino-m-hydroxypropiophenone methiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 95605-39-3
3-(dimethylamino)-1-(3-hydroxyphenyl)propan-1-one

: 74-88-4
methyl iodide

: 76106-42-8
β-dimethylamino-m-hydroxypropiophenone methiodide

Guidance literature:: In diethyl ether; at 10 ℃; for 12h;
DOI:10.1039/P19800001555

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 76106-42-8
β-dimethylamino-m-hydroxypropiophenone methiodide

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / conc. aq. HCl / ethanol / 48 h / Heating

2: 27 percent / diethyl ether / 12 h / 10 °C

With hydrogenchloride; In diethyl ether; ethanol;
DOI:10.1039/P19800001555

Reference yield:

: 5453-62-3
β-dimethylamino-m-hydroxypropiophenone hydrochloride

: 76106-42-8
β-dimethylamino-m-hydroxypropiophenone methiodide

Guidance literature:: Multi-step reaction with 3 steps

1: 2.9 percent / NaOH / H₂O / 0.67 h / Heating

2: 72 percent / conc. aq. HCl / ethanol / 48 h / Heating

3: 27 percent / diethyl ether / 12 h / 10 °C

With hydrogenchloride; sodium hydroxide; In diethyl ether; ethanol; water;
DOI:10.1039/P19800001555