2-(2,4,6-trimethylphenyl)-2H-benzo[d]imidazo-[5,1-b]thiazol-9-ylium trifluoromethanesulfonate

Base Information

• Chemical Name: 2-(2,4,6-trimethylphenyl)-2H-benzo[d]imidazo-[5,1-b]thiazol-9-ylium trifluoromethanesulfonate
• CAS No.: 1061178-56-0
• Molecular Formula: CF₃O₃S*C₁₈H₁₇N₂S
• Molecular Weight: 442.483

Synonyms:2-(2,4,6-trimethylphenyl)-2H-benzo[d]imidazo-[5,1-b]thiazol-9-ylium trifluoromethanesulfonate

Chemical Property of 2-(2,4,6-trimethylphenyl)-2H-benzo[d]imidazo-[5,1-b]thiazol-9-ylium trifluoromethanesulfonate

Chemical Property:

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Technology Process of 2-(2,4,6-trimethylphenyl)-2H-benzo[d]imidazo-[5,1-b]thiazol-9-ylium trifluoromethanesulfonate

There total 1 articles about 2-(2,4,6-trimethylphenyl)-2H-benzo[d]imidazo-[5,1-b]thiazol-9-ylium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

Chloromethyl pivalate (18997-19-8) + [(E)-1-(benzothiazol-2-yl)methylidene]-2,4,6-trimethylphenylamine (1061178-54-8) + silver trifluoromethanesulfonate (2923-28-6) → 2-(2,4,6-trimethylphenyl)-2H-benzo[d]imidazo-[5,1-b]thiazol-9-ylium trifluoromethanesulfonate (1061178-56-0)

Guidance literature:

Chloromethyl pivalate; silver trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 0.75h; Darkness;

[(E)-1-(benzothiazol-2-yl)methylidene]-2,4,6-trimethylphenylamine; In dichloromethane; at 40 ℃; for 16h; Darkness;

DOI:10.1055/s-2008-1067147

Reference yield: 83.0%

2-(2,4,6-trimethylphenyl)-2H-benzo[d]imidazo-[5,1-b]thiazol-9-ylium trifluoromethanesulfonate (1061178-56-0) → 2-(2,4,6-trimethylphenyl)-2H-benzo[d]imidazo[5,1-b]thiazole-1-thione (1061178-60-6)

Guidance literature:

With potassium tert-butylate; sulfur; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1055/s-2008-1067147

Reference yield:

2-(2,4,6-trimethylphenyl)-2H-benzo[d]imidazo-[5,1-b]thiazol-9-ylium trifluoromethanesulfonate (1061178-56-0) → C18H16N2S (1061178-59-3)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran-d8; at 20 ℃; for 0.0833333h;

DOI:10.1055/s-2008-1067147

upstream raw materials:

Chloromethyl pivalate

[(E)-1-(benzothiazol-2-yl)methylidene]-2,4,6-trimethylphenylamine

silver trifluoromethanesulfonate

Downstream raw materials:

C₁₈H₁₆N₂S

2-(2,4,6-trimethylphenyl)-2H-benzo[d]imidazo[5,1-b]thiazole-1-thione

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