Acetic acid,2-(4-nitrophenoxy)-,2-[1,2-dihydro-1-[[4-(4-methylphenyl)-1-piperazinyl]methyl]-2-oxo-3H-indol-3-ylidene]hydrazide

Base Information

• Chemical Name: Acetic acid,2-(4-nitrophenoxy)-,2-[1,2-dihydro-1-[[4-(4-methylphenyl)-1-piperazinyl]methyl]-2-oxo-3H-indol-3-ylidene]hydrazide
• CAS No.: 81215-60-3
• Molecular Formula: C₂₈H₂₈N₆O₅
• Molecular Weight: 528.568

Synonyms:Aceticacid, (4-nitrophenoxy)-,[1,2-dihydro-1-[[4-(4-methylphenyl)-1-piperazinyl]methyl]-2-oxo-3H-indol-3-ylidene]hydrazide(9CI)

Chemical Property of Acetic acid,2-(4-nitrophenoxy)-,2-[1,2-dihydro-1-[[4-(4-methylphenyl)-1-piperazinyl]methyl]-2-oxo-3H-indol-3-ylidene]hydrazide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.36g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetic acid,2-(4-nitrophenoxy)-,2-[1,2-dihydro-1-[[4-(4-methylphenyl)-1-piperazinyl]methyl]-2-oxo-3H-indol-3-ylidene]hydrazide

There total 3 articles about Acetic acid,2-(4-nitrophenoxy)-,2-[1,2-dihydro-1-[[4-(4-methylphenyl)-1-piperazinyl]methyl]-2-oxo-3H-indol-3-ylidene]hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + (4-methylphenyl)piperazine (39593-08-3) + (4-Nitro-phenoxy)-acetic acid [2-oxo-1,2-dihydro-indol-(3Z)-ylidene]-hydrazide (81215-48-7) → (4-Nitro-phenoxy)-acetic acid [2-oxo-1-(4-p-tolyl-piperazin-1-ylmethyl)-1,2-dihydro-indol-(3Z)-ylidene]-hydrazide (81215-60-3)

Guidance literature:

In ethanol;

DOI:10.1002/ardp.19823150207

Reference yield:

(4-nitro-phenoxy)-acetic acid hydrazide (75129-74-7) → (4-Nitro-phenoxy)-acetic acid [2-oxo-1-(4-p-tolyl-piperazin-1-ylmethyl)-1,2-dihydro-indol-(3Z)-ylidene]-hydrazide (81215-60-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / glacial acetic acid / ethanol / Heating

2: 70 percent / ethanol

With acetic acid; In ethanol;

DOI:10.1002/ardp.19823150207

Reference yield:

indole-2,3-dione (91-56-5,1186480-61-4,84788-92-1) → (4-Nitro-phenoxy)-acetic acid [2-oxo-1-(4-p-tolyl-piperazin-1-ylmethyl)-1,2-dihydro-indol-(3Z)-ylidene]-hydrazide (81215-60-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / glacial acetic acid / ethanol / Heating

2: 70 percent / ethanol

With acetic acid; In ethanol;

DOI:10.1002/ardp.19823150207

upstream raw materials:

formaldehyd

(4-methylphenyl)piperazine

(4-Nitro-phenoxy)-acetic acid [2-oxo-1,2-dihydro-indol-(3Z)-ylidene]-hydrazide

(4-nitro-phenoxy)-acetic acid hydrazide

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