6a-(4-methoxyphenyl)-5H-benzo[4,5][1,3]oxazino[2,3-a]isoindole-5,11(6aH)-dione

Base Information

Chemical Name:6a-(4-methoxyphenyl)-5H-benzo[4,5][1,3]oxazino[2,3-a]isoindole-5,11(6aH)-dione
CAS No.:908-65-6
Molecular Formula:C₂₂H₁₅NO₄
Molecular Weight:357.365
Hs Code.:

Synonyms:6a-(4-methoxyphenyl)-5H-benzo[4,5][1,3]oxazino[2,3-a]isoindole-5,11(6aH)-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6a-(4-methoxyphenyl)-5H-benzo[4,5][1,3]oxazino[2,3-a]isoindole-5,11(6aH)-dione

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Technology Process of 6a-(4-methoxyphenyl)-5H-benzo[4,5][1,3]oxazino[2,3-a]isoindole-5,11(6aH)-dione

There total 4 articles about 6a-(4-methoxyphenyl)-5H-benzo[4,5][1,3]oxazino[2,3-a]isoindole-5,11(6aH)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1022-46-4
2-phenyl-4H-3,1-benzoxazin-4-one

: 123-11-5
4-methoxy-benzaldehyde

: 579-93-1
2-(Benzoylamino)benzoic Acid

: 908-65-6
6a-(4-methoxyphenyl)-5H-benzo[4,5][1,3]oxazino[2,3-a]isoindole-5,11(6aH)-dione

Guidance literature:: With tert.-butylhydroperoxide; palladium diacetate; In 1,4-dioxane; water; at 120 ℃; for 18h; Sealed tube;
DOI:10.1002/ejoc.201800263

Reference yield: 62.0%

: 18600-55-0
2-(4-methoxyphenyl)-4H-3,1-benzoxazin-4-one

: 611-73-4
Benzoylformic acid

: 908-65-6
6a-(4-methoxyphenyl)-5H-benzo[4,5][1,3]oxazino[2,3-a]isoindole-5,11(6aH)-dione

Guidance literature:: With ammonium persulfate; palladium diacetate; silver nitrate; In 1,2-dichloro-ethane; at 120 ℃; for 18h;
DOI:10.1002/adsc.201901142

Reference yield: 52.0%

: 104-93-8
p-methylanizole

: 1022-46-4
2-phenyl-4H-3,1-benzoxazin-4-one

: 579-93-1
2-(Benzoylamino)benzoic Acid

: 908-65-6
6a-(4-methoxyphenyl)-5H-benzo[4,5][1,3]oxazino[2,3-a]isoindole-5,11(6aH)-dione

Guidance literature:: With tert.-butylhydroperoxide; palladium diacetate; In water; at 120 ℃; for 18h; Sealed tube;
DOI:10.1002/ejoc.201800263